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ADZ Laboratories, Inc. <br /> 2773 Downhill Drive Steamboat Springs, CO 80487(800)334-5493 <br /> HCltasca Denver, Inc. ACZ Sample ID: L43424-01 <br /> Project ID: CCV_4059-3 Date Sampled: 1 112911 7 00:00 <br /> Sample ID: B12-PHASE 2 Date Received: 03/29/18 <br /> Sample Matrix: Soil <br /> Soil Preparation <br /> Parameter EPA Method Dilution Result Qual XQ Units MDL Date Analyst <br /> Air Dry at 34 Degrees USDA No.1,1972 04/02/18 10:38 ajm <br /> C <br /> Crush and Pulverize EPA-600/2-78-054 3.1.3 04/03/18 10:38 ajm <br /> (Ring&Puck) <br /> Digestion-Hot Plate M3050B ICP 04/04/18 13:37 ajm <br /> Digestion-Hot Plate M3050B ICP-MS 04/04/18 13:37 ajm <br /> Meteoric Water ASTM E2242-13 <br /> Mobility Extraction <br /> Dry Weight 1 5000 g 04/06/18 0:00 dbt <br /> Extraction pH 1 5.23 units 04/06/18 0:00 dbt <br /> Extraction 1 23.0 C 0.1 0.1 04/06/18 0:00 dbt <br /> Temperature <br /> Extraction Time 1 27 hrs 04/06/18 0:00 dbt <br /> Leachate Volume 1 5000 mL 04/06/18 0:00 dbt <br /> Particle Size over 5 1 0 % 04/06/18 0:00 dbt <br /> cm <br /> Post Filter pH 1 4.69 units 04/06/18 0:00 dbt <br /> Pre Filter pH 1 4.71 units 04/06/18 0:00 dbt <br /> Retained Moisture 1 11.34 % 04/06/18 0:00 dbt <br /> Temperature 1 21.7 C 0.1 0.1 04/06/18 0:00 dbt <br /> Time In 1 04/06/18 0:00 dbt <br /> Time Out 1 04/06/18 0:00 dbt <br /> Wet Chemistry <br /> MethodParameter EPA Dilution Result Qual XQ Units MDL PQL Date Analyst <br /> Alkalinity(MWMT) SM2320B-Titration <br /> Bicarbonate as 1 U * mg/L 2 20 04/17/18 0:00 the <br /> CaCO3 <br /> Carbonate as CaCO3 1 U mg/L 2 20 04/17/18 0:00 the <br /> Hydroxide as CaCO3 1 U mg/L 2 20 04/17/18 0:00 the <br /> Total Alkalinity 1 U mg/L 2 20 04/17/18 0:00 the <br /> Chloride(MWMT) SM4500CI-E 1 1.4 B mg/L 0.5 2 04/17/18 11:27 jmm <br /> Cyanide,WAD SM4500-CN 1,E- 0.5 UH mg/L 0.003 0.01 04/17/18 15:05 kea <br /> (MWMT) Colorimetric w/distillation <br /> Fluoride(MWMT) SM450OF-C 20 2 B * mg/L 1 5 04/19/18 12:41 emk <br /> Nitrate/Nitrite as N M353.2-Automated 1 0.74 H mg/L 0.02 0.1 04/10/18 23:25 pjb <br /> (MWMT) Cadmium Reduction <br /> Nitrogen,total Kjeldahl M351.2-Block Digestor 1 0.3 B mg/Kg 0.1 0.5 04/21/18 20:30 pjb <br /> (MWMT) <br /> Residue, Filterable SM2540C 1 268 * mg/L 10 20 04/12/18 16:09 the <br /> (TDS)@180C <br /> (MWMT) <br /> Sulfate(MWMT) D516-07-Turbidimetric 5 186 mg/L 5 25 04/16/18 13:21 jmm <br /> REPIN.02.06.05.01 'Please refer to Qualifier Reports for details. <br /> L43424-1805031420 Page 6 of 47 <br />