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ACZ Laboratories, Inc. • • • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Alexco Water& Environmental Inc. ACZ Project ID: L53488 <br /> METHODACZ ID WORKNUM PARAMETER <br /> L53488-01 NG478037 Cyanide,WAD SM4500-CN I,E-Colorimetric wl 06 Sample was received above recommended temperature. <br /> distillation <br /> SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the.concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG479202 Fluoride SM450OF-C Q6 Sample was received above recommended temperature. <br /> WG479075 Nitrate/Nitrite as N M353.2-H2SO4 preserved Q6 Sample was received above recommended temperature. <br /> M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG478702 Phosphorus,total M365.1-Auto Ascorbic Acid Q6 Sample was received above recommended temperature. <br /> (digest) <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG478042 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature. <br /> SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG477993 Residue,Non-Filterable(TSS)@105C SM2540D Q6 Sample was received above recommended temperature. <br /> SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG479255 Total Hot Plate Digestion M200.2 ICP-MS DJ Sample dilution required due to insufficient sample. <br /> L53488-02 NG478037 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ Q6 Sample was received above recommended temperature. <br /> distillation <br /> SM4500-CN I,E-Colorimetric wl RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1Ox MDL). <br /> WG479202 Fluoride SM450OF-C Q6 Sample was received above recommended temperature. <br /> WG479075 Nitrate/Nitrite as N M353.2-H2SO4 preserved Q6 Sample was received above recommended temperature. <br /> M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MIX). <br /> W G478702 Phosphorus,total M365.1-Auto Ascorbic Acid Q6 Sample was received above recommended temperature. <br /> (digest) <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG478042 Residue,Filterable(TDS)@180C SM2540C 06 Sample was received above recommended temperature. <br /> SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG477993 Residue,Non-Filterable(TSS)@105C SM2540D Q6 Sample was received above recommended temperature. <br /> SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG479255 Total Hot Plate Digestion M200.2 ICP-MS DJ Sample dilution required due to insufficient sample. <br /> REPAID.15.06.05.01 <br /> L53488-1908160933 Page 11 of 21 <br />