2019-05-29_PERMIT FILE - M2019031 ‎(7)‎

• Permit No: M2019031
• IBM Index Class Name: Permit File
• Doc Date: 5/29/2019
• Doc Name: Application
• From: Atlas Mining and Reclamation LLC
• To: DRMS
• Email Name: THM
• Media Type: D
• Archive: No

ADZ Laboratories, Inc. • • • - •
2773 Downhill Drive Steamboat Springs, CO 80487 [phone] - • •
eardon Steel LLC ACZ Project ID: L49791
METHODACZ ID WORKNUM PARAMETER QUAL DESCRIPTION
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1Ox MDL)
WG466717 Iron,total(3050) M6010D ICP M3 The spike recovery value is unusable since the analyte
concentration in the sample is disproportionate to the spike
level The recovery of the associated control sample(LCS
or LFB)was acceptable
WG466578 Lead(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466896 Lead,total(3050) M6020B ICP-MS MA Recovery for either the spike or spike duplicate was outside
of the acceptance limits,the RPD was within the
acceptance limits
M6020B ICP-MS ZH Serial Dilution exceeded the acceptance criteria Matrix
interference[physical or chemical]is suspected
WG466546 Magnesium(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
Manganese(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466753 Manganese,total(3050) M6010D ICP M3 The spike recovery value is unusable since the analyte
concentration in the sample is disproportionate to the spike
level The recovery of the associated control sample(LCS
or LFB)was acceptable
WG466902 Mercury(1312) M7470A CVAA RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<10x MDL)
WG466716 Neutralization Potential as CaCO3 M600/2-78-054 3 2 3 RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466546 Nickel(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
Potassium(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466578 Selenium(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<10x MDL)
WG466546 Silver(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<10x MDL)
Sodium(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<10x MDL)
WG466388 Sulfate(1312 DI) D516-07-Turbidimetric HD Analysis is outside the intended scope of the method,which
does not provide hold time information for soil extracts No
hold time is observed for collection to extraction The
referenced method hold time is observed for extraction-to-
analysis
D516-07-Turbidimetric M1 Matrix spike recovery was high,the recovery of the
associated control sample(LCS or LFB)was acceptable
D516-07-Turbidimetric RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466649 Sulfur Pyritic Sulfide M600/2-78-054 3 2 4 RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
Sulfur Sulfate M600/2-78-054 3 2 4 RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466578 Thallium(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
WG466896 Thallium,total(3050) M6020B ICP-MS D1 Sample required dilution due to matrix
WG466708 Total Alkalinity SM2320B-Titration RA Relative Percent Difference(RPD)was not used for data
validation because the concentration of the duplicated
sample is too low for accurate evaluation(<1 Ox MDL)
REPAD.15.06.05.01
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