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Ar"Z Laboratories, Inc. • - • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Ouray Silver Mines ACZ Project 1D: L48502 <br /> METHOD:ACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> Nickel(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG463544 Ndrate/Nitrite as N(1312-DI) M353.2-Automated Cadmium HD Analysis is outside the intended scope of the method, <br /> Reduction wtuc h does not provide hold time information for soil <br /> extracts. No hold time is observed for collection to <br /> extraction- The tellereloed method hold time is observed <br /> for extradion4o-analysis. <br /> M353.2-Automated Cadmium 06 Sample was received above recommended temperature. <br /> Reduction <br /> M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was rat used for data <br /> Reduction validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> Nitrite as N(1312-DI) M3532-Automated Cadmium HD Analysis is outside the intended scope of the method, <br /> Reduction which does not provide told time information for soil <br /> eh. . - No told time is observed for collection to <br /> extraction. The referenced method told time is observed <br /> for extraction-to-anaws. <br /> M3532-Automated Cadmium C16 Sample was received above recommended temperature. <br /> Reduction <br /> M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was not used for data <br /> Reduction validation because the concentratim of the duplicated <br /> sample is too low for accurate evalluaWn(<10x MOIL). <br /> WG463471 Nitrogen,ammonia(1312-DI) M350.1 Auto Salicylate w/gas HD Analysis is outside the intended scope of the method, <br /> diffusion W is h does not provide told lime inliom agon for soil <br /> extracts- No hold time is observed for collection to <br /> extraction. The referenced method told time is observed <br /> for extraction-to-analysis. <br /> M350.1 Auto Salicylate wlgas 06 Sample was received above recommended temperature. <br /> diffusion <br /> M350.1 Auto Salicylate w/gas RA Relative Percent Difference(RPD)was not used for data <br /> diffusion validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG463542 Phosphorus,ortho dissolved(1312-DI) M365.1-Automated Ascorbic HD Analysis is outside the intended scope of the method, <br /> Acid which does not provide hold time information for soil <br /> extracts. No hold time is observed for collection to <br /> extraction. The referenced method told time is observed <br /> for extract c to-analysis. <br /> M365.1-Automated Ascorbic RA Relative Percent Difference(RPD)was not used for data <br /> Acid validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> W G463643 Phosphorus,Total(1312-DI) M365.1-Auto Ascorbic Acid HD Analysis is outside the intended scope of the method, <br /> (digest) which does not provide hold time intormation for soil <br /> extracts. No hold time is observed for collection to <br /> extraction. The referenced method hold time,is observed <br /> for extraction-to-analysis- <br /> kMA-Auto Ascorbic Acid RA Relative Percent Differerre(R^D)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> W G463420 Potassium(1312) M6010D ICP RA Relative Percent Difference(RPD)was rot used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> W G463519 Residue.Filerable(TDS)Q180C(1312) SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG463492 Selenium(1312) M6020B ICP-VS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concerhtration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> Silver(1312) M6020B ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the corcentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG463420 Sodium(1312) M6010D ICP RA Relative Percent Difference(RPD)was not used for data <br /> vMdabon because the concentration of the duplicated <br /> sample is Soo low for accurate evaluation(<1 Ox MDL). <br /> Strontium(1312) W10D ICP RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> REPAD.15.06.05.01 <br /> L48502-1901031643 Page 24 of 32 <br />