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ACZ Laboratories, Inc. • • - • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Ouray Silver Miffs ACZ Project ID: L48502 <br /> METHODIACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MIDI-). <br /> Nickel(1312) M602W ICP-MS RA Relative Percent Difference(RPD)was not used for data <br /> validation because the eormcerdraian of the drpicaled <br /> sample is too bar for accurate ecru rV" _ ,— ._.:.. <br /> W G463544 NdtatelNitrite as N(1312-0I) M353.2-Automated Cadmium HD Analysis is outside the intended scope of the method, <br /> Reuiucbm which does not provide hold time information for soil <br /> extracts- No hold Erne is observed for Collection to <br /> "^•+" - Tv mel od hold tine is observed <br /> L43532-Automated Cadmium Q6 Sam*was received above reccrnrnended temperature. <br /> Reduction <br /> M3532-Ardor+-Aed Cadmium RA►. Relative Percent Difference(RID)was not used for data <br /> Reduction vaid4�c^.:______ <br /> sample is too low for aecu-le evaluation(<1 Ox MDL). <br /> Nitrite as N(1312-01) M3532-Automated Cadmium HID Analysis is outside the intended scope of the method, <br /> Reduction which does not provide hold time intimation for soil <br /> tetrads No hold time is observed for collection to <br /> .. ...ciiwau hard finis is Observed <br /> for ems. <br /> M353.2-Automated Cadmium 06 Sample was received above recommended temperature. <br /> Reduction <br /> M3532-Automated Cadmium RA Relative Percent Difference(RPD)was riot used for data <br /> Reduction validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG463471 Nitrogen,ammo is(1312-0I) M350-1 Auk Saicylate WVas HID Analysis is oulaide the intended scope of the method, <br /> diffusion which does rot provide hold time information for soil <br /> e)&acts- No hold time is observed for collection to <br /> extraction. The referenced method hold time is observed <br /> for . <br /> M350.1 Auto SaRcylate w00as 06 Sample was received above recommended temperature. <br /> diffusion <br /> M350.1 Auto Saikytate wlgas RA Relative Percent Difference(RPD)was not used for data <br /> dillusion validation because fie conowhaion of the duplicated <br /> sample is too low for acc ra/e evaluation(<1 Ox MDL). <br /> _. -._-•_ -- --_--__; ._-; .:"....-'-sated Ascorbic HD Analysis is outside the intended scope of the method, <br /> Acid which does rot provide hold time information for sou! <br /> extracts. No told lime is observed for collection to <br /> exbacdiom The referenced method hold time is observed <br /> for extractia►-to-aralysis. <br /> LM-1-Aulormafed Ascorbic RA Relative Percent Dittorence(RPD)was not used for data <br /> Acid validation because tare concentration of the duplicated <br /> sample is too tow for accu are evaluation(<10x MDL). <br /> DI) .....t.."..:carbic Acid HD Analysis is outside the intended scope of the method, <br /> (digest) which does not provide hold time information for soil <br /> extracts. No told fire is observed for collection to <br /> extracian_ The referenced mhed hold time is observed <br /> for <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Ddlererce(RPD)was not used fox data <br /> (digest) vaidaron because the eoroentrabon of the duplicated <br /> sample is too low for acaurale evaluation(<1 Ox MDL). <br /> _.__. <br /> validation be cat the concentration of the duplicated <br /> sample is too tow for accurate evaluation(<1(x MDL). <br /> WG463519 Residue.Filterable(rDS)@180C(1312) SM2540C RA Relative Percent Difference(RPD)was not <br /> validation bcc=;--- ._ <br /> samples too tow for accurate evaluation(<10x ILL). <br /> WG463492 Selenium(1312) MfXM ICP4AS RA Relative Percent lire ce(RPD)was not used for data <br /> - rn because the concentration of the duplicated <br /> - - --�— �- -----�- - -�---- ." _....•.ate). <br /> SWei-(1312) M6020t3)cP-MS RA Relative Percent Difference(RPD)was riot used for data <br /> vaidabon because the concemYabon of the dupicaled <br /> sample is too tow for accurate evokabon(<10x MDL} <br /> W - - - - - hr-.-.._.. _ Re. -- <br /> vaidabon because the caoumtation of the duplicated <br /> sample is too tow for aaaaaile evaluation(<10x MDL). <br /> c.....+:.o rt zt?) ...,..,...n ro ... ..-• --^- ..:�.........._,rraorik-:w not used for data <br /> -d <br /> L48502-1901031643 Page 21 of 32 <br />