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Batch ID:16-97223 to 16-97224 WS# <br />Internal Standard:0.1 ml 25-037-13 Serial Dilution:5 fold U-238 MDL Bi-209 IS: <br />Total Volume:10 ml LRB:0.1/10 25-037-13 U-238 MDL Ir-193 IS: <br />LCS:0.25/10 of 25-037-04 expected 25 µg/L ICSA:25-038-06 Mo-98 MDL In-115 IS: <br />Spike:0.25/10 of 25-037-04 expected 25 µg/L ICSAB:25-038-07 <br />1 CB 25-037-13 Cal Blk 100.0% <br />2 C1 25-037-14 1ppb 1.000 104.8% <br />3 C2 25-037-15 5ppb 4.999 106.8% <br />4 C3 25-037-16 10ppb 10.027 107.4% <br />5 C4 25-038-01 20ppb 20.014 108.2% <br />6 C5 25-038-02 50ppb 49.948 106.6% <br />7 C6 25-038-03 100ppb 99.949 110.2% <br />8 C7 25-038-04 200ppb 199.883 107.0% <br />9 ICV 25-038-05 100ppb 103.607 108.2% <br />10 ICB 0.001 103.0% <br />11 ICSA 25-038-06 100 ppb 109.424 102.5% <br />12 ICSAB 25-038-07 2 ppb 2.250 101.4% <br />13 ICSAB 25-038-07 2 ppb 2.261 104.1% <br />14 LRB Lab Reagent Blank 10.00 1 0.00066 0.01165 103.1% <br />15 LCS 25 ppb Spike 10.00 1 26.457 0.01165 107.3% <br />16 Method Blank #2 Prep Blank N/A 0.05 200 0.363 2.33000 107.8%1500 12.0476 0.12 0.045 <br />17 16-97223 CARTFIL-ASH 27-Oct-16 0.05 200 2167.139 2.33000 106.4%1500 8.7779 0.17 370.329 <br />18 16-97223 D Dup (CARTFIL-ASH)0.05 200 2159.850 2.33000 103.3%1500 8.7779 0.17 369.083 <br />19 16-97223 SD Serial Dilution (CARTFIL-ASH)0.05 200 421.464 2.33000 104.1%1500 8.7779 0.17 72.021 <br />20 16-97223 MS Matrix Spike (CARTFIL-ASH)0.05 200 7559.006 2.33000 102.9%1500 8.7779 0.17 1291.711 <br />21 CCV 100ppb 100.811 115.2% <br />22 CCB -0.001 108.1% <br />23 16-97224 R/OMEMB-ASH 27-Oct-16 0.05 200 1472.382 2.33000 102.7%1500 12.0476 0.12 183.321 <br />24 CCV 100ppb 98.821 108.9% <br />25 CCB -0.001 107.5% <br />Sample Result <br />Sample Result <br />QC <br />QC <br />QC <br />QC <br />0.01067 µg/L <br />0.01165 µg/L <br />0.1404 µg/L <br />ICP-MS <br />Dilution <br />Factor <br />Schwartzwalder Special Request Column and R/O Analysis: U- <br />238 & Mo-98 <br />U-238 <br />(µg/L)RDL (µg/L) <br />Ir-193 <br />Recovery <br />(%) <br />Ir-193 Internal Standard <br />Final <br />Volume <br />(mL) <br />Sample <br />Mass (g) <br />Volume/ <br />Mass <br />(L/g) <br />Pipettes:MS9, MS2, MS10, 31, MS8 <br />Notes <br />Date of Analysis: 11/04/16 <br />#Lab #Location/ <br />Description <br />Collectio <br />n Date <br />Aliquot <br />Volume <br />(mL)U-238 <br />(µg/g) <br />Calculated Results <br />V:\Data\Lab.Data\2016\11\Schwartz Mine\ICP-MS\Special Request\Schwartwalder Special Request Column and RO-U-Mo 16-97223 to 16-97224 (11-04-16)Page 1