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ADZ Laboratories, Inc. • • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 Al - • • <br /> Ouray Silver Mines ACZ Project ID: L43205 <br /> L4320"3 AIG443637 Chloride SM4500CI-E M2 Matrix spike recovery was low,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable. <br /> WG443975 Cyanide,total M335 4-Colonmetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG443710 Fluoride SM450OF-C M2 Matrix spike recovery was low,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable <br /> WG443574 Phosphorus,ortho dissolved M365 1-Automated Ascorbic QP The sample was filtered at the laboratory more than 15 <br /> Acid minutes after sample collection. For Orthophosphate,40 <br /> CFR Part 136.3 requires filtration within 15 minutes of <br /> collection <br /> M365.1-Automated Ascorbic RA Relative Percent Difference(RPD)was not used for data <br /> Acid validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> M365.1-Automated Ascorbic ZU Analysis date/time preceeds filter date/time. A portion of <br /> Acid sample was filtered and analyzed prior to the creation of a <br /> Filter workgroup <br /> WG443581 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG443646 Silver,dissolved M200.8 ICP-MS M2 Matrix spike recovery was low,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable <br /> M200.8 ICP-MS RF Relative Percent Difference(RPD)for Ag in spiked <br /> samples exceeded limit. In the absence of HCI, <br /> precipitation of Ag may occur at different rates <br /> WG443528 Sulfate D516-02/-07-Turbidimetnc M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable <br /> REPAD.15.06.05.01 <br /> L43205-1803231004 Page 18 of 22 <br />