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soCrgrtGroup Analytical Report 2 of 11 <br /> Client: Cotter Corp <br /> Analyte: Chloride <br /> Prep Date: 10/13/2017 <br /> Analysis Date: 10/13/2017 <br /> Approved Method Source: 40 CFR 136.3 <br /> Prep ID: SM 4500-CI--1997 <br /> Analytical Method ID: SM 4500-CI--1997 <br /> Instrument: Titrimetric <br /> Matrix: Aqueous(water,wastewater,groundwater) <br /> Sample volume used: 100 mL <br /> Analyst: SE <br /> Location ID SmaDate SCG# Results Flags RL Units <br /> MINE REFILL 10/11/17 317697.A 18 2 mg/L <br /> Client: Cotter Corp <br /> Analyte: Sulfate,SOT <br /> Prep Date: 10/19/20 t 7 <br /> Analysis Date: 10/19/2017 <br /> Approved Method Source: 40 CFR 136.3 <br /> Prep ID: ASTM D516-07 <br /> Analytical Method ID: ASTM D516-07 <br /> Instrument: Evo 160,UVNIS <br /> Matrix: Aqueous(water,wastewater,groundwater) <br /> Sample volume used: 100 mL Dilution Factor: 50 <br /> Analyst: SE <br /> Location ID Smn Date SCG# Results Flags MDL RL Units <br /> MINE REFILL 10/11/17 31769TA 1,622 6.0 29.5 mg/L <br /> Qualifiers: <br /> E—Extrapolated value.Value exceeds calibration range <br /> H—Analysis exceeded holding time <br /> J—Estimated value detected below the RL/MRL <br /> S—Spike recovery outside acceptance limits <br /> U—Analyte not detected <br /> X—See case narrative Confidential and Privileged 10-Nov-17 <br />