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ADZ Laboratories, Inc. • • - • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Ouray Silver Mines ACZ Project ID: L37780 <br /> ACZ JD .. <br /> L37780-01 NG425418 Cyanide,total M335 4-Colon metric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425103 Fluoride SM450OF-C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG425246 Nitrate/Nitrite as N M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG424796 Phosphorus,ortho dissolved M365 1-Automated Ascorbic Acid HE Analysis performed past holding time Method holding time <br /> is less than or equal to 7 days and sample was received <br /> with less than half of the holding time remaining(refer to <br /> item C5 of ACZ's Terms&Conditions) <br /> M365 1-Automated Ascorbic Acid M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable <br /> WG424886 Residue,Non-Filterable(fSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425368 Sulfate D516-02/-07-Turbidimetric M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable <br /> L37780-02 NG425418 Cyanide,total M335 4-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425103 Fluoride SM450OF-C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425246 Nitrate/Nitrite as N M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG424796 Phosphorus,ortho dissolved M365 1-Automated Ascorbic Acid HE Analysis performed past holding time Method holding time <br /> is less than or equal to 7 days and sample was received <br /> with less than half of the holding time remaining(refer to <br /> item C5 of ACZ's Terms&Conditions) <br /> M365 1-Automated Ascorbic Acid M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable <br /> WG424886 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> L37780-03 NG425100 Chloride SM4500CI-E RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425418 Cyanide,total M335 4-Colon metric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425103 Fluoride SM450OF-C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG425246 Nitrate/Nitrite as N M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG424796 Phosphorus,ortho dissolved M365 1-Automated Ascorbic Acid HE Analysis performed past holding time Method holding time <br /> is less than or equal to 7 days and sample was received <br /> with less than half of the holding time remaining(refer to <br /> item C5 of ACZ's Terms&Conditions) <br /> M365 1-Automated Ascorbic Acid M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable <br /> WG424886 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> REPAD.15.06.05.01 <br /> L37780-1706271658 Page 17 of 21 <br />