2017-08-07_GENERAL DOCUMENTS - M2017003

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Laboratories, Inc. -- -- 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 Lewicki &Associates ACZ Project 1D. L37726 L37726-01 NG426309 Acid Generation Potential(talc) M600/2-78-054 1 3 N1 See Case Narrative Acid Neutralization Potential(talc) M600/2-78-054 1 3 N1 See Case Narrative. Acid-Base Potential(talc) M600/2-78-054 1.3 N1 See Case Narrative WG426040 Aluminum total(3050) M6010B ICP M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level The recovery of the associated control sample(LCS or LFB)was acceptable. ING426215 Boron,total(3050) M60108 ICP 61 Target analyte detected in prep/method blank at or above the method reporting limit See Case Narrative M60108 ICP M2 Matrix spike recovery was low,the recovery of the associated control sample(LCS or LFB)was acceptable M60108 ICP ZG The ICP or ICP-MS Serial Dilution was not used for data validation because the sample concentration was less than 50 times the MDL. WG426134 Carbon,total(TO) ASA No 9 29-Z2 4 CombustiONIR Q6 Sample was received above recommended temperature ASA No.9 29-2 2.4 Combustion/IR RA Relative Percent Difference(RPD)was not used for data validation because the concentration of the duplicated sample is too low for accurate evaluation(<10x MDL). Carbon,total inorganic(TIC) ASA No.9 29-2 2.4(talc TO- Q6 Sample was received above recommended temperature. TOO) ASA No.9 29-2.2.4(talc TO- RA Relative Percent Difference(RPD)was not used for data TOC) validation because the concentration of the duplicated sample is too low for accurate evaluation(<1 Ox MDL) ASA No.9 29-2 2 4(talc TO- ZQ Analyte was not evaluated in the laboratory control TOC) standard. Either the analyte is not inducted in the scope of the analytical method or a commercial standard containing the analyte is not available Carbon,total organic(TOC) ASA No 9 29-2 2 4 Combustion/iR Q6 Sample was received above recommended temperature ASA No 9 29-2.2 4 Combustion/lR RA Relative Percent Difference(RPD)was not used for data validation because the concentration of the duplicated sample is too low for accurate evaluation(<1 Ox MDL), ASA No 9 29-2 2.4 CombustionrlR ZQ Analyte was not evaluated in the laboratory control standard. Either the analyte is not included in the scope of the analytical method or a commercial standard containing the analyte is not available WG426040 Cobalt total(3050) M6010B ICP ZG The ICP or ICP-MS Serial Dilution was not used for data validation because the sample concentration was less than 50 times the MDL WG426215 Copper total(3050) M6010B ICP M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportonate to the spike level.The recovery of the associated control sample(LCS or LFB)was acceptable VIJG426142 Iron,total(3050) M6010B ICP N13 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level.The recovery of the associated control sample(LCS or LFB)was acceptable. WG426215 Lead,total(3050) M60106 ICP M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level.The recovery of the associated control sample(LCS or LFB)was acceptable. Manganese,total(3050) M6010B ICP M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level.The recovery of the associated control sample(LCS or LFB)was acceptable WG425510 Mercury total M7471A CVAA Q6 Sample was received above recommended temperature WG426040 Molybdenum.total(3050) N16010B ICP ZG The ICP or ICP-MS Serial Dilution was not used for data validation because the sample concentration was less than 50 times the MDL Phosphorus total(3050) M60106 ICP M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level.The recovery of the associated control sample(LCS or LFB)was acceptable WG426099 Sulfur Organic Residual M600/2-78-054 3 2 4-MOD RA Relative Percent Difference(RPD)was not used for data validation because the concentration of the duplicated sample is too low for accurate evaluation(<1 Ox MDL) Sulfur Sulfate M600/2-78-054 3 2 n-MOD R1 RPD exceeded the method or laboratory acceptance limit REPAD.15.06.05.01 L37726-1707261644 Pine 14 c4: 10