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ADZ Laboratories, Inc. • - - • <br /> ' 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Golder Associates ACZ Project ID: L37566 <br /> ' . ER METH067777 <br /> L37566-07 NG424199 Bicarbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> Carbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG425180 Chloride M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> ' sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG424199 Hydroxide as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> pH SM4500H+B Q6 Sample was received above recommended temperature <br /> SM4500H+B ZW Method deviation The sample was centrifuged prior to <br /> analysis due to high solid content <br /> pH measured at SM4500H+B Q6 Sample was received above recommended temperature <br /> WG424116 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG425180 Sulfate M300 0-Ion Chromatography DC Sample required dilution Non-target analyte exceeded <br /> calibration range <br /> M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> WG424199 Total Alkalinity SM2320B-Titration Q6 Sample was received above recommended temperature <br /> SM2320B-Titration ZW Method deviation The sample was centrifuged prior to <br /> analysis due to high solid content <br /> L37566-08 NG424199 Bicarbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG424692 Calcium,dissolved M200 7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG424199 Carbonate as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG425180 Chloride M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> M300 0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> ' WG424199 Hydroxide as CaCO3 SM2320B-Titration Q6 Sample was received above recommended temperature <br /> WG424692 Iron,dissolved M200 7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable <br /> WG424760 Manganese,dissolved M200 7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable <br /> ' WG424199 pH SM4500H+B Q6 Sample was received above recommended temperature <br /> pH measured at SM4500H+B Q6 Sample was received above recommended temperature <br /> WG424116 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG425180 Sulfate M300 0-Ion Chromatography Q6 Sample was received above recommended temperature <br /> ' WG424199 Total Alkalinity SM2320B-Titration Q6 Sample was received above recommended temperature <br /> REPAID 15.06.05.01 <br /> ' L37566-1706221642 Page 17 of 23 <br />