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Lab Numbers: 20161121701 - 20161121706 Page 7 <br />QC <br />Smp <br />Parameter Lab# <br />Value <br />Value <br />Spike DF <br />Result <br />Limits <br />Method <br />Continuing Calibration Verification <br />Zinc - D <br />0.049 <br />0.050 <br />1 <br />-1.4246 <br />(-8.583) - (3.595) <br />EPA 200.8 <br />Bismuth <br />0.052 <br />0.050 <br />1 <br />3.4096 <br />(-7.448) - (13.72) <br />EPA 200.8 <br />Bismuth <br />0.052 <br />0.050 <br />1 <br />4.20% <br />(-7.448) - (13.72) <br />EPA 200.8 <br />Bismuth <br />0.052 <br />0.050 <br />1 <br />4.20% <br />(-7.448) - (13.72) <br />EPA 200.8 <br />Gold - T <br />0.082 <br />0.075 <br />1 <br />9.73% <br />(-12.10) - (19.60) <br />EPA 231.2 <br />Gold - T <br />0.110 <br />0.100 <br />1 <br />9.90P6 <br />(-12.10) - (19.60) <br />EPA 231.2 <br />Mercury - T <br />0.0021 <br />0.0020 <br />1 <br />3.50% <br />(-7.650) - (5.710) <br />EPA 245.1 <br />Mercury - T <br />0.0052 <br />0.0050 <br />1 <br />4.00% <br />(-7.650) - (5.710) <br />EPA 245.1 <br />Mercury - T <br />0.0010 <br />0.0010 <br />1 <br />-2.00% <br />(-7.850) - (5.710) <br />EPA 245.1 <br />Tellurium <br />0.051 <br />0.050 <br />1 <br />1.80% <br />(-12.14) - (9.642) <br />EPA 200.8 <br />Tellurium <br />0.051 <br />0.050 <br />1 <br />1.80% <br />(-12.14) - (9.642) <br />EPA 200.8 <br />Tellurium <br />0.050 <br />0.050 <br />1 <br />-1.004 <br />(-12.14) - (9.642) <br />EPA 200.8 <br />Titanium - T <br />0.050 <br />0.050 <br />1 <br />0.00% <br />(-7.406) - (6.806) <br />EPA 200.8 <br />Titanium - T <br />0.050 <br />0.050 <br />1 <br />-0.200% <br />(-7.406) - (6.806) <br />EPA 200.8 <br />Titanium -T <br />0.050 <br />0.050 <br />1 <br />-0.400% <br />(-7.406) - (6.806) <br />EPA 200.8 <br />Zirconium <br />0.050 <br />0.050 <br />1 <br />-0.600% <br />(-10.79) - (11.39) <br />EPA 200.8 <br />Zirconium <br />0.050 <br />0.050 <br />1 <br />-0.600% <br />(-10.79) - (11.39) <br />EPA 200.8 <br />Zirconium <br />0.049 <br />0.050 <br />1 <br />-2.20% <br />(-10.79) - (11.39) <br />EPA 200.8 <br />Gold - TCLP <br />0.112 <br />0.100 <br />1 <br />11.6 % <br />EPA 231.2 <br />Gold - TCLP <br />0.082 <br />0.075 <br />1 <br />9.73% <br />EPA 231.2 <br />Initial Calibration Blank <br />Antimony - D <br />0.000 <br />0.00 <br />1 <br />0.00021 <br />(-0.0008) - (0.0018) <br />EPA 200.8 <br />Beryllium - D <br />0.000 <br />0.00 <br />1 <br />0.00003 <br />(-0.0002) - (0.0005) <br />EPA 200.8 <br />Cadmium - D <br />0.000 <br />0.00 <br />1 <br />0.00005 <br />(-0.0001) - (0.0001) <br />EPA 200.8 <br />Cobalt - D <br />0.000 <br />0.00 <br />1 <br />0.00002 <br />EPA 200.8 <br />Molybdenum - D <br />0.000 <br />0.00 <br />1 <br />0.00004 <br />(-0.0002) - (0.0004) <br />EPA 200.8 <br />Nickel - D <br />0.000 <br />0.00 <br />1 <br />0.00006 <br />(-0.0001) - (0.0001) <br />EPA 200.8 <br />Selenium - D <br />0.000 <br />0.00 <br />1 <br />0.00018 <br />(-0.0001) - (0.0003) <br />EPA 200.8 <br />Silver - D <br />0.000 <br />0.00 <br />1 <br />0.00004 <br />(0.0000) - (0.0001) <br />EPA 200.8 <br />Bismuth <br />0.000 <br />0.00 <br />1 <br />0.00002 <br />EPA 200.8 i <br />Gold - T <br />0.000 <br />0.00 <br />1 <br />0.00015 <br />(-0.0003) - (0.0004) <br />EPA 231.2 <br />Mercury - T <br />0.0000 <br />0.000 <br />1 <br />0.00001 <br />(-0.0001) - (0.0001) <br />EPA 245.1 <br />Tellurium <br />0.000 <br />0.00 <br />1 <br />0.00004 <br />EPA 200.8 <br />Titanium - T <br />0.000 <br />0.00 <br />1 <br />0.00001 <br />EPA 200.8 <br />Zirconium <br />0.000 <br />0.00 <br />1 <br />0.00003 <br />EPA 200.8 <br />Gold - TCLP <br />0.000 <br />0.00 <br />1 <br />-0.00005 <br />EPA 231.2 <br />Continuing Calibration Blank <br />Aluminum - D <br />0.000 <br />0.00 <br />1 <br />0.00003 <br />(-0.0003) - (0.0005) <br />EPA 200.8 <br />Arsenic - D <br />0.000 <br />0.00 <br />1 <br />0.00005 <br />(-0.0001) - (0.0001) <br />EPA 200.8 <br />Arsenic - D <br />0.000 <br />0.00 <br />1 <br />0.00004 <br />(-0.0001) - (0.0001) <br />EPA 200.8 <br />Barium - D <br />0.000 <br />0.00 <br />1 <br />0.00003 <br />(0.0000) - (0.0001) <br />EPA 200.8 <br />Cadmium - D <br />0.000 <br />0.00 <br />1 <br />0.00001 <br />(0.0000) - (0.0001) <br />EPA 200.8 <br />Calcium - D <br />0.040 <br />0.00 <br />1 <br />0.04 <br />(-0.3291) - (0.3733) <br />SM 3111 B <br />Calcium - D <br />0.050 <br />0.00 <br />1 <br />0.05 <br />(-0.3291) - (0.3733) <br />SM 3111 B : <br />