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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />New Elk Coal Co., LLC ACZ Sample ID: <br />L33796-01 <br />Project ID: Date Sampled: <br />10/26/16 14:40 <br />Sample ID: PRS 1 Date Received: <br />10/27/16 <br />Sample Matrix: <br />Surface Water <br />Inorganic Prep <br />Acidify and filter Colorado 5 CCR 1002- 10/28/16 15:50 scp <br />(Potentially Dissolved) 31.5.31 (2009) <br />Total Hot Plate M200.2 ICP 11/01/16 12:45 gss <br />Digestion <br />Total Recoverable M200.2 ICP 11/02/16 16:30 gss <br />Digestion <br />Metals Analysis <br />REPIN.02.06.05.01 , Please refer to Qualifier Reports for details - <br />L33796 -1611080847 Page 2 of 12 <br />3r777M <br />ra] <br />XQ Units <br />MDL) <br />- <br />Calcium, dissolved <br />M200.7 ICP <br />1 <br />40.4 <br />mg/L <br />0.1 <br />0.5 <br />11/07/16 14:39 <br />gss <br />Iron, dissolved <br />M200.7 ICP <br />1 <br />0.04 <br />B <br />mg/L <br />0.02 <br />0.05 <br />11/07/16 14:39 <br />gss <br />Iron, total <br />M200.7 ICP <br />1 <br />0.09 <br />mg/L <br />0.02 <br />0.05 <br />11/02/16 20:24 <br />gss <br />Iron, total recoverable <br />M200.7 ICP <br />1 <br />0.09 <br />mg/L <br />0.02 <br />0.05 <br />11/03/16 13:38 <br />gss <br />Magnesium, dissolved <br />M200.7 ICP <br />1 <br />6.4 <br />mg/L <br />0.2 <br />1 <br />11/07/16 14:39 <br />gss <br />Manganese, dissolved <br />M200.7 ICP <br />1 <br />0.008 <br />B <br />mg/L <br />0.005 <br />0.03 <br />11/07/16 14:39 <br />gss <br />Manganese, total <br />M200.7 ICP <br />1 <br />0.014 <br />B <br />mg/L <br />0.005 <br />0.03 <br />11/02/16 20:24 <br />gss <br />Potassium, dissolved <br />M200.7 ICP <br />1 <br />1.2 <br />mg/L <br />0.2 <br />1 <br />11/07/16 14:39 <br />gss <br />Selenium, potentially <br />M200.8 ICP -MS <br />1 <br />0.0002 <br />B <br />mg1L <br />0.0001 <br />0.0003 <br />11/02/16 9:50 <br />mfm <br />dissolved <br />Sodium, dissolved <br />M200.7 ICP <br />1 <br />5.1 <br />mg/L <br />0.2 <br />1 <br />11/07/16 14:39 <br />gss <br />REPIN.02.06.05.01 , Please refer to Qualifier Reports for details - <br />L33796 -1611080847 Page 2 of 12 <br />