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I�(A. dzufelt@greenanalytical.com p: 970.247.4220 f: 970.247.4227 75 Suttle Street Durango, CO 81303 <br />Laboratories www.GreenAnalytical.com <br />GCC Energy, LLC Project: GCC GW Baseline <br />6473 CR 120 Project Name / Number: [none] Reported: <br />Hesperus CO, 81326 Project Manager: Tom Bird 10/19/16 17:49 <br />General Chemistry - Quality Control <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch B609183 - General Prep - Wet Chem <br />Blank (B609183-BLK1) Prepared & Analyzed: 09/23/16 <br />Alkalinity, Total ND 10.0 mgCaCO3/L <br />LCS (B609183-BS1) Prepared & Analyzed: 09/23/16 <br />Alkalinity, Total 103 10.0 mgCaCO3/L 100 103 85-115 <br />LCS Dup (B609183-BSD1) Prepared & Analyzed: 09/23/16 <br />Alkalinity, Total 104 10.0 mgCaCO3/L 100 104 85-115 0.966 20 <br />Batch B609199 - General Prep - Wet Chem <br />Blank (B609199-BLK1) <br />Prepared: 09/27/16 Analyzed: 09/28/16 <br />Chloride <br />ND <br />1.00 <br />mg/L <br />Fluoride <br />ND <br />0.100 <br />mg/L <br />Sulfate <br />ND <br />1.00 <br />mg/L <br />LCS (B609199-BS1) <br />Prepared & Analyzed: 09/27/16 <br />Chloride <br />24.6 <br />1.00 <br />mg/L 25.0 98.3 <br />90-110 <br />Fluoride <br />2.49 <br />0.100 <br />mg/L 2.50 99.7 <br />90-110 <br />Sulfate <br />24.7 <br />1.00 <br />mg/L 25.0 98.6 <br />90-110 <br />LCS Dup (B609199-BSD1) <br />Prepared & Analyzed: 09/27/16 <br />Chloride <br />24.4 <br />1.00 <br />mg/L 25.0 97.4 <br />90-110 0.858 20 <br />Fluoride <br />2.47 <br />0.100 <br />mg/L 2.50 98.9 <br />90-110 0.806 20 <br />Sulfate <br />24.4 <br />1.00 <br />mg/L 25.0 97.6 <br />90-110 1.03 20 <br />Batch B609205 - General Prep - Wet Chem <br />Blank (B609205-BLK1) Prepared & Analyzed: 09/26/16 <br />Total Dissolved Solids ND 10.0 mg/L <br />Duplicate (B609205-DUPl) Source: 1609173-01 Prepared & Analyzed: 09/26/16 <br />Total Dissolved Solids 370 10.0 mg/L 370 0.00 20 <br />Reference (B609205-SRMl) Prepared: 09/26/16 Analyzed: 09/28/16 <br />Total Dissolved Solids 405 mg/L 400 101 85-115 <br />Batch B609216 - General Prep - Wet Chem <br />Duplicate (B609216-DUPl) Source: 1609188-01 Prepared & Analyzed: 09/22/16 <br />pH 7.29 pH Units 7.29 0.00 20 <br />Green Analytical Laboratories <br />Debbie Zufelt, Reports Manager <br />The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALS liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing and received within <br />thirty days after completion of the applicable service. <br />Page 7 of 20 <br />