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l(A. dzufelt@greenanalytical.com p: 970.247.4220 f: 970.247.4227 75 Suttle Street Durango, CO 81303 <br />Laboratories www.GreenAnalytical.com <br />GCC Energy, LLC Project: GCC GW & SW Baseline <br />6473 CR 120 Project Name / Number: GCC Energy LLC Reported: <br />Hesperus CO, 81326 Project Manager: Tom Bird 08/08/16 11:32 <br />General Chemistry - Quality Control <br />(Continued) <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch B606247 - General Prep - Wet Chem (Continued) <br />Reference (B606247-SRMl) (Continued) Prepared & Analyzed: 06/27/16 <br />Total Dissolved Solids 375 10.0 mg/L 400 93.8 85-115 <br />Batch B606260 - General Prep - Wet Chem <br />Blank (B606260-BLK1) Prepared & Analyzed: 06/28/16 <br />Total Suspended Solids ND 2.00 -9/1- <br />Duplicate <br />g/L <br />Duplicate (B606260-DUPl) Source: 1606260-05 Prepared & Analyzed: 06/28/16 <br />Total Suspended Solids 18.5 2.00 mg/L 18.0 2.74 20 <br />Reference (B606260-SRMl) Prepared & Analyzed: 06/28/16 <br />Total Suspended Solids 96.0 2.00 mg/L 100 96.0 85-115 <br />Batch B606261 - General Prep - Wet Chem <br />Blank (B606261-BLKl) Prepared & Analyzed: 07/01/16 <br />Chloride ND 1.00 mg/L <br />Fluoride ND 0.100 mg/L <br />Sulfate ND 1.00 mg/L <br />LCS (B606261-BS1) Prepared & Analyzed: 07/01/16 <br />Chloride 24.2 1.00 mg/L 25.0 96.6 90-110 <br />Fluoride 2.47 0.100 mg/L 2.50 98.8 90-110 <br />Sulfate 24.1 1.00 mg/L 25.0 96.3 90-110 <br />LCS Dup (B606261-BSD1) Prepared & Analyzed: 07/01/16 <br />Chloride 24.3 1.00 mg/L 25.0 97.0 90-110 0.413 20 <br />Fluoride 2.45 0.100 mg/L 2.50 98.2 90-110 0.650 20 <br />Sulfate 24.3 1.00 mg/L 25.0 97.2 90-110 0.930 20 <br />Batch B607007 - General Prep - Wet Chem <br />Blank (B607007-BLK1) <br />Prepared & Analyzed: 07/05/16 <br />Nitrate/Nitrite as N <br />ND 0.020 mg/L <br />LCS (B607007-BS1) <br />Prepared & Analyzed: 07/05/16 <br />Nitrate/Nitrite as N <br />1.01 0.020 mg/L 1.00 101 90-110 <br />LCS Dup (B607007-BSD1) <br />Prepared & Analyzed: 07/05/16 <br />Nitrate/Nitrite as N <br />- - - - - - - - - - - - - - - <br />1.01 0.020 mg/L 1.00 101 90-110 0.338 20 <br />- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - <br />Green Analytical Laboratories <br />Debbie Zufelt, Reports Manager <br />The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALS liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing and received within <br />thirty days after completion of the applicable service. <br />Page 16 of 30 <br />