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Inorganic Extended <br /> ACZ Laboratories, Inc. g <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 Qualifier Report <br /> Golder Associates ACZ Project ID: L28976 <br /> ACZ ID WORKNUM PARAMETER METHOD QUAL DESCRIPTION <br /> L28976-05 WG398723 Calcium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> Magnesium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG398831 Chloride M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> L28976-06 WG398723 Calcium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> Magnesium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG398831 Chloride M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG398662 pH SM4500H+B ZW Method deviation. The sample was centrifuged prior to <br /> analysis due to high solid content. <br /> WG398831 Sulfate M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> WG398662 Total Alkalinity SM2320B-Titration ZW Method deviation. The sample was centrifuged prior to <br /> analysis due to high solid content. <br /> L28976-07 WG398723 Calcium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> Magnesium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG398831 Chloride M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> Sulfate M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> REPAD.15.06.05.01 <br /> L28976-1602251543 Page 16 of 21 <br />