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AALS <br />ANALYTICAL REPORT <br />W orkorder: 34-1604403 <br />Client Project ID: Twenty Mile Coal 021216 <br />Purchase Order: NA <br />Project Manager: Paul Pope <br />Analytical Results <br />Sample ID: SP -1 <br />Lab ID: 1604403001 <br />Analyst <br />Collected: 02/12/2016 <br />Received: 02/13/2016 <br />Method: NIOSH 7903 <br />Sampling <br />Media: Liquid Analyzed: 02/15/2016 <br />Parameter: Volume Not Provided <br />Analyte <br />Result (ug/g) <br />RL (ug/g) <br />Fluoride <br /><5.0 <br />5.0 <br />Chloride <br />190 <br />5.0 <br />Bromide <br /><5.0 <br />5.0 <br />Nitrate Ion <br /><5.0 <br />5.0 <br />Phosphate Ion <br /><5.0 <br />5.0 <br />Sulfate <br />3800 <br />50 <br />Comments <br />Sample: 1604403001 <br />NIOSH 7300 Mod.: A 15 mL aliquot of sample was digested and analyzed for metals by ICP. <br />NIOSH 7300 Mod.: The sodium result for this sample is reported from 2X dilution data in order to obtain an instrument result <br />within the linear range for sodium. The reporting limit has been raised by the dilution factor. <br />Report Authorization (/S/ is an electronic signature that complies with 21 CFR Part 11) <br />Method <br />Analyst <br />Peer Review <br />/S/ John M. Reynolds <br />/S/ Thomas J. Masoian <br />IH by GC -MS Scan <br />02/16/2016 16:09 <br />02/16/2016 16:17 <br />/S/ Peter P. Steen <br />/S/ Lauren Jones <br />NIOSH 7300 Mod. <br />02/16/2016 14:43 <br />02/16/2016 16:35 <br />/S/ John Carpenter <br />/S/ Christopher Winter <br />NIOSH 7903 <br />02/16/2016 14:25 <br />02/16/2016 15:00 <br />Laboratory Contact Information <br />ALS Environmental <br />960 W Levoy Drive <br />Salt Lake City, Utah 84123 <br />Phone: (801) 266-7700 <br />Email: alslt.lab@ALSGlobal.com <br />Web: www.alsslc.com <br />Page 2 of 3 Tue, 02/16/16 4:42 PM IHREP-V12.2 <br />