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Analytical dzufelt@greenanalytical.comp: 970.247.4220 f: 970.247.4227 75 Suttle Street Durango, CO 81303 <br />Laboratories <br />www.GreenAnalytical.com <br />GCC Energy, LLC Project: King I & King II <br />6473 CR 120 Project Name / Number: King I & King II Reported: <br />Hesperus CO, 81326 Project Manager: Tom Bird 07/09/15 12:27 <br />Wiltze Well <br />King I <br />1506220-01 (Wai <br />Analyte Result RL VLDL Units Dilution Analyzed Method Notes Analyst <br />General Chemist <br />Alkalinity, <br />Bicarbonate* <br />450 <br />10.0 <br />mg/L <br />5 <br />07/07/15 <br />2320 B <br />LLG <br />Alkalinity, <br />Carbonate* <br /><10.0 <br />10.0 <br />mg/L <br />5 <br />07/07/15 <br />2320 B <br />LLG <br />Alkalinity, <br />Hydroxide* <br /><10.0 <br />10.0 <br />mg/L <br />5 <br />07/07/15 <br />2320 B <br />LLG <br />Alkalinity, <br />Total* <br />450 <br />10.0 <br />mg/L <br />5 <br />07/07/15 <br />2320 B <br />LLG <br />PH* <br />1.47 <br />7.35 <br />0.0007 <br />pH Units <br />1 <br />06/25/15 <br />EPA150.1 <br />114 MJV <br />TDS* <br />90.8 <br />1430 <br />10.0 <br />mg/L <br />1 <br />06/29/15 <br />EPA160.1 <br />ABP <br />Sulfate <br />555 <br />100 <br />16.8 mg/L <br />10 <br />07/07/15 <br />4500-SO42- E <br />ABP <br />Dissolved Metals by ICP <br />Calcium* <br />193 <br />0.020 <br />0.003 <br />mg/L <br />1 <br />06/25/15 <br />EPA200.7 <br />JGS <br />Hardness <br />986 <br />0.462 <br />0.140 <br />mgCaCO3/L <br />1 <br />06/25/15 <br />2340 B <br />JGS <br />Iron* <br /><0.050 <br />0.050 <br />0.003 <br />mg/L <br />1 <br />06/25/15 <br />EPA200.7 <br />JGS <br />Magnesium* <br />123 <br />0.100 <br />0.032 <br />mg/L <br />1 <br />06/25/15 <br />EPA200.7 <br />JGS <br />Manganese* <br />1.47 <br />0.005 <br />0.0007 <br />mg/L <br />1 <br />06/25/15 <br />EPA200.7 <br />JGS <br />Sodium* <br />90.8 <br />1.00 <br />0.305 <br />mg/L <br />1 <br />06/25/15 <br />EPA200.7 <br />JGS <br />CGreen Analytical Laboratories <br />Debbie Zufelt, Reports Manager <br />The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALS liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing andreceived within <br />thirty days after completion of the applicable service. <br />Page 3 of 12 <br />