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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Twentymile Coal Co. <br />ACZ Project ID: L27265 <br />ID WORKNUM PARAMETER <br />L27265-01 WG392922 *All Compounds* <br />METHODACZ <br />M8015D GC/FID <br />QUAL <br />Q6 <br />DESCRIPTION <br />Sample was received above recommended temperature. <br />TPH C10 to C28 <br />M8015D GC/FID <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG392697 *All Compounds* <br />M8015D GC/FID <br />D1 <br />Sample required dilution due to matrix. <br />M8015D GC/FID <br />Q2 <br />Sample received with head space. <br />M8015D GC/FID <br />Q6 <br />Sample was received above recommended temperature. <br />M8015D GC/FID <br />Q9 <br />Insufficient sample received to meet method QC <br />requirements. <br />WG392688 <br />M8260B GC/MS <br />D1 <br />Sample required dilution due to matrix. <br />M8260B GC/MS <br />Q2 <br />Sample received with head space. <br />M8260B GC/MS <br />Q6 <br />Sample was received above recommended temperature. <br />M8260B GC/MS <br />Q9 <br />Insufficient sample received to meet method QC <br />requirements. <br />L27265-02 WG392923 *All Compounds* <br />M8015D GC/FID <br />Q6 <br />Sample was received above recommended temperature. <br />M8015D GC/FID <br />Q9 <br />Insufficient sample received to meet method QC <br />requirements. <br />OTP <br />M8015D GC/FID <br />S13 <br />Surrogate recovery was below laboratory and method <br />acceptance limits. See Case Narrative. <br />WG392956 *All Compounds* <br />M8015D GC/FID <br />D1 <br />Sample required dilution due to matrix. <br />M8015D GC/FID <br />Q2 <br />Sample received with head space. <br />M8015D GC/FID <br />Q6 <br />Sample was received above recommended temperature. <br />M8015D GC/FID <br />Q9 <br />Insufficient sample received to meet method QC <br />requirements. <br />WG392687 <br />M8260B GC/MS <br />Q6 <br />Sample was received above recommended temperature. <br />M8260B GC/MS <br />Q9 <br />Insufficient sample received to meet method QC <br />requirements. <br />R E PA D.15.06.05.01 <br />L27265-1510261048 Page 19 of 23 <br />