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rte, <br />Laboratories, Inc. <br />Twentymile Coal Co. ACZ Project ID: L27265 <br />VINYL ACETATE <br />VINYL CHLORIDE <br />BROMOFLUOROBENZENE (surr) <br />DIBROMOFLUOROMETHANE (surr) <br />TOLUENE -D8 (surr) <br />25 <br />25.2 <br />25.95 <br />21.81 <br />ug/L <br />ug/L <br />% <br />% <br />% <br />104.0 <br />86.0 <br />96.1 <br />104.0 <br />109.1 <br />70 <br />70 <br />70 <br />70 <br />70 <br />130 <br />130 <br />130 <br />130 <br />130 <br />LCSWD Sample ID: WG392687LCSWD <br />Compound QC Sample <br />PCN/SCN: V161016-4-CCV <br />Found Units <br />Rec <br />Lower <br />Analyzed: <br />Upper RPD <br />10/20/15 13:00 <br />Limit Qual <br />1,1,1,2 -TETRACHLOROETHANE <br />25.1 <br />23.33 <br />ug/L <br />93.0 <br />70 <br />130 <br />8 <br />20 <br />1,1,1 -TRICHLOROETHANE <br />25.1 <br />26.98 <br />ug/L <br />108.0 <br />70 <br />130 <br />1 <br />20 <br />1,1,2,2 -TETRACHLOROETHANE <br />24.9 <br />28.27 <br />ug/L <br />113.0 <br />70 <br />130 <br />14 <br />20 <br />1,1,2 -TRICHLOROETHANE <br />25 <br />23.68 <br />ug/L <br />95.0 <br />70 <br />130 <br />14 <br />20 <br />1,1-DICHLOROETHANE <br />24.9 <br />25.28 <br />ug/L <br />102.0 <br />70 <br />130 <br />6 <br />20 <br />1,1-DICHLOROETHENE <br />25 <br />21.54 <br />ug/L <br />86.0 <br />70 <br />130 <br />14 <br />20 <br />1,1-DICHLOROPROPENE <br />25.2 <br />25.35 <br />ug/L <br />101.0 <br />70 <br />130 <br />9 <br />20 <br />1,2,3-TRICHLOROBENZENE <br />25.1 <br />26.9 <br />ug/L <br />107.0 <br />70 <br />130 <br />17 <br />20 <br />1,2,3-TRICHLOROPROPANE <br />25.1 <br />26.68 <br />ug/L <br />106.0 <br />70 <br />130 <br />11 <br />20 <br />1,2,4-TRICHLOROBENZENE <br />25 <br />26.3 <br />ug/L <br />105.0 <br />70 <br />130 <br />12 <br />20 <br />1,2,4-TRIMETHYLBENZENE <br />25.1 <br />25.22 <br />ug/L <br />101.0 <br />70 <br />130 <br />4 <br />20 <br />1,2-DIBROMO-3-CHLOROPROPANE <br />24.9 <br />28.15 <br />ug/L <br />113.0 <br />70 <br />130 <br />15 <br />20 <br />1,2-DIBROMOETHANE <br />25.1 <br />23.52 <br />ug/L <br />94.0 <br />70 <br />130 <br />12 <br />20 <br />1,2 -DICHLOROBENZENE <br />24.5 <br />26.99 <br />ug/L <br />110.0 <br />70 <br />130 <br />10 <br />20 <br />1,2-DICHLOROETHANE <br />25.2 <br />24.58 <br />ug/L <br />98.0 <br />70 <br />130 <br />11 <br />20 <br />1,2-DICHLOROPROPANE <br />25.1 <br />26.64 <br />ug/L <br />106.0 <br />70 <br />130 <br />10 <br />20 <br />1,3,5-TRIMETHYLBENZENE <br />24.9 <br />25.97 <br />ug/L <br />104.0 <br />70 <br />130 <br />4 <br />20 <br />1,3 -DICHLOROBENZENE <br />24.7 <br />24.68 <br />ug/L <br />100.0 <br />70 <br />130 <br />2 <br />20 <br />1,3-DICHLOROPROPANE <br />25 <br />24.08 <br />ug/L <br />96.0 <br />70 <br />130 <br />15 <br />20 <br />1,4 -DICHLOROBENZENE <br />24.7 <br />25.1 <br />ug/L <br />102.0 <br />70 <br />130 <br />2 <br />20 <br />2,2-DICHLOROPROPANE <br />25 <br />26.86 <br />ug/L <br />107.0 <br />70 <br />130 <br />0 <br />20 <br />2-BUTANONE <br />50.1 <br />51.33 <br />ug/L <br />103.0 <br />70 <br />130 <br />9 <br />20 <br />2-CHLOROTOLUENE <br />24.7 <br />25.11 <br />ug/L <br />102.0 <br />70 <br />130 <br />3 <br />20 <br />2-HEXANONE <br />50 <br />53.56 <br />ug/L <br />107.0 <br />70 <br />130 <br />18 <br />20 <br />4-CHLOROTOLUENE <br />24.7 <br />25.49 <br />ug/L <br />103.0 <br />70 <br />130 <br />4 <br />20 <br />4-ISOPROPYLTOLUENE <br />25 <br />25.53 <br />ug/L <br />102.0 <br />70 <br />130 <br />1 <br />20 <br />4-METHYL-2-PENTANONE <br />50 <br />51.45 <br />ug/L <br />103.0 <br />70 <br />130 <br />14 <br />20 <br />ACETONE <br />50 <br />39.5 <br />ug/L <br />79.0 <br />70 <br />130 <br />11 <br />20 <br />ACRYLONITRILE <br />25 <br />23.95 <br />ug/L <br />96.0 <br />70 <br />130 <br />1 <br />20 <br />BENZENE <br />25 <br />24.06 <br />ug/L <br />96.0 <br />70 <br />130 <br />7 <br />20 <br />BROMOBENZENE <br />25.1 <br />27.77 <br />ug/L <br />111.0 <br />70 <br />130 <br />13 <br />20 <br />BROMOCHLOROMETHANE <br />24.9 <br />24.96 <br />ug/L <br />100.0 <br />70 <br />130 <br />3 <br />20 <br />BROMODICHLOROMETHANE <br />24.6 <br />24.87 <br />ug/L <br />101.0 <br />70 <br />130 <br />2 <br />20 <br />BROMOFORM <br />25.2 <br />23.86 <br />ug/L <br />95.0 <br />70 <br />130 <br />2 <br />20 <br />BROMOMETHANE <br />25 <br />21.61 <br />ug/L <br />87.0 <br />70 <br />130 <br />6 <br />20 <br />CARBON DISULFIDE <br />25.3 <br />21.29 <br />ug/L <br />84.0 <br />70 <br />130 <br />14 <br />20 <br />CARBON TETRACHLORIDE <br />25.1 <br />25.44 <br />ug/L <br />101.0 <br />70 <br />130 <br />6 <br />20 <br />CHLOROBENZENE <br />24.8 <br />24.1 <br />ug/L <br />97.0 <br />70 <br />130 <br />3 <br />20 <br />CHLOROETHANE <br />25 <br />20.96 <br />ug/L <br />84.0 <br />70 <br />130 <br />21 <br />20 R1 <br />CHLOROFORM <br />25 <br />23.96 <br />ug/L <br />96.0 <br />70 <br />130 <br />8 <br />20 <br />CHLOROMETHANE <br />25.1 <br />20.83 <br />ug/L <br />83.0 <br />70 <br />130 <br />16 <br />20 <br />L27265-1510261048 Page 15 of 23 <br />