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The approved laboratory2 provides NS with pre -cleaned and pre -preserved sample bottles. In <br />addition, the laboratory handles the QA/QC protocols for all groundwater samples. NS <br />conducts all field sampling, field data collection, and sample collection. NS is responsible for <br />ensuring groundwater samples are delivered to the laboratory within the required hold times <br />and preservation techniques. Daub performs additional QA/QC by compiling all analytical data <br />and cross checking the data with historical values. <br />3.2 Field Measurements and Calibration <br />General methodologies for field measurements are located in Appendix B, Sections B.9 through <br />B.13. Calibration of field instrumentation will be conducted according to manufacturer's <br />recommendations, refer to Table 2 for basic calibration checks. If calibration acceptance <br />criteria are not met during the operational check, a primary calibration of the affected probe(s) <br />and instruments(s) must be conducted. Probe replacement or cleaning may also be required if <br />the operational acceptance criteria are not met, per the manufacturer's calibration <br />specifications. <br />Parameter <br />Requirement <br />Frequency <br />Operational Check <br />Criteria <br />pH <br />Three-point calibration <br />Prior to start of <br />sampling event <br />NA <br />One -point check <br />Prior to start of <br />sampling event <br />±0.2pH <br />unit <br />Specific <br />Conductance <br />One -point calibration <br />Prior to start of <br />sampling event <br />NA <br />One -point operational <br />check <br />Prior to start of <br />sampling event <br />±10% of standard <br />Temperature <br />NA <br />NA <br />NA <br />Table 2. Field Equipment Calibration Checks <br />4 Sample Identification and Handling Procedures <br />Each sample will be assigned an identifier that corresponds to each well name or surface <br />sample location. In addition, a unique Project ID will be assigned to each sample group <br />analyzed by the laboratory (See Section B.2, "Standard Practice for Sample Labeling," in <br />2 ACZ Laboratories, Inc. in Steamboat Springs, CO is currently contracted to NS for water sample <br />analyses. <br />Daub & Associates, Inc. 6 NS LLC 2015 S A P Rev. 2 <br />