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• �\\ Trust our People. Trust our Data. Billings, MT 800 735.4489 • Casper, WY 888.135.0515 <br />,ww.ene gylab.con, College Station, TX 888.690 2218 • Gillette, WY 866 686.7175 • Helena. MT 877.472.0711 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: <br />Cotter Corporation <br />Report Date: <br />06/02/15 <br />Project: <br />Schwartz - SW 5/1/15 S27880, S27882 <br />Work Order: <br />C15050078 <br />Analyte <br />Count Result Units <br />RL %REC Low Limit High Limit RPD <br />RPDLimit Qual <br />Method: E200.8 <br />Lab ID: MB -44633 <br />7 <br />Method Blank <br />Analytical Run: ICPMS4-C_150521A <br />Lab ID: ICV <br />7 Initial Calibration Verification Standard <br />Arsenic <br />ICPMS4-C <br />05/21/15 15:56 <br />Antimony <br />0.0496 <br />mg/L <br />0.0010 <br />99 <br />90 <br />110 <br />Arsenic <br />0.0504 <br />mg/L <br />0.0010 <br />101 <br />90 <br />110 <br />Chromium <br />0.0502 <br />mg/L <br />0.0010 <br />100 <br />90 <br />110 <br />Copper <br />0.0511 <br />mg/L <br />0.0010 <br />102 <br />90 <br />110 <br />Lead <br />0.0480 <br />mg/L <br />0.0010 <br />96 <br />90 <br />110 <br />Molybdenum <br />0.0489 <br />mg/L <br />0.0010 <br />98 <br />90 <br />110 <br />Thallium <br />0.0476 <br />mg/L <br />0.0010 <br />95 <br />90 <br />110 <br />Method: E200.8 <br />Lab ID: MB -44633 <br />7 <br />Method Blank <br />Antimony <br />ND mg/L <br />Arsenic <br />ICPMS4-C <br />ND mg/L <br />Chromium <br />05/21/1518:22 <br />ND mg/L <br />Copper <br />0.0005 mg/L <br />Lead <br />ND mg/L <br />Molybdenum <br />ND mg/L <br />Thallium <br />6E-05 mg/L <br />Lab ID: LCS3-44633 <br />7 <br />Laboratory Control Sample <br />Antimony <br />0.540 mg/L <br />Arsenic <br />0.502 mg/L <br />Chromium <br />0.478 mg/L <br />Copper <br />0.477 mg/L <br />Lead <br />0.513 mg/L <br />Molybdenum <br />0.494 mg/L <br />Thallium <br />0.0002 <br />0.452 mg/L <br />Lab ID: C15050134-003AMS3 <br />7 <br />Sample Matrix Spike <br />Antimony <br />0.518 mg/L <br />Arsenic <br />0.506 mg/L <br />Chromium <br />0.466 mg/L <br />Copper <br />0.470 mg/L <br />Lead <br />150521A <br />0.496 mg/L <br />Molybdenum <br />0.0010 <br />0.469 mg/L <br />Thallium <br />85 <br />0.458 mg/L <br />Lab ID: C15050134-003AMSD <br />7 <br />Sample Matrix Spike Duplicate <br />Antimony <br />0.527 mg/L <br />Arsenic <br />0.526 mg/L <br />Chromium <br />96 <br />0.480 mg/L <br />Copper <br />115 <br />0.492 mg/L <br />Lead <br />0.0050 <br />0.510 mg/L <br />Molybdenum <br />85 <br />0.478 mg/L <br />Thallium <br />0.466 mg/L <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 17 of 31 <br />Batch: 44633 <br />Run: <br />ICPMS4-C <br />150521A <br />05/21/1518:22 <br />0.0002 <br />0.0004 <br />0.0003 <br />0.0002 <br />4E-05 <br />0.0002 <br />6E-05 <br />Run: <br />ICPMS4-C <br />150521A <br />05/21/1518:27 <br />0.0010 <br />108 <br />85 <br />115 <br />0.0010 <br />100 <br />85 <br />115 <br />0.0050 <br />96 <br />85 <br />115 <br />0.0050 <br />95 <br />85 <br />115 <br />0.0010 <br />103 <br />85 <br />115 <br />0.0010 <br />99 <br />85 <br />115 <br />0.00050 <br />90 <br />85 <br />115 <br />Run: <br />ICPMS4-C <br />150521A <br />05/21/1519:03 <br />0.0010 <br />104 <br />70 <br />130 <br />0.0010 <br />101 <br />70 <br />130 <br />0.0050 <br />93 <br />70 <br />130 <br />0.0050 <br />93 <br />70 <br />130 <br />0.0010 <br />99 <br />70 <br />130 <br />0.0010 <br />94 <br />70 <br />130 <br />0.00050 <br />92 <br />70 <br />130 <br />Run: <br />ICPMS4-C_150521A <br />05/21/1519:08 <br />0.0010 <br />105 <br />70 <br />130 <br />1.6 <br />20 <br />0.0010 <br />105 <br />70 <br />130 <br />4.0 <br />20 <br />0.0050 <br />96 <br />70 <br />130 <br />3.1 <br />20 <br />0.0050 <br />98 <br />70 <br />130 <br />4.5 <br />20 <br />0.0010 <br />102 <br />70 <br />130 <br />2.7 <br />20 <br />0.0010 <br />96 <br />70 <br />130 <br />1.9 <br />20 <br />0.00050 <br />93 <br />70 <br />130 <br />1.8 <br />20 <br />ND - Not detected at the reporting limit. <br />Page 17 of 31 <br />