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Trust our People. Trust our Data. Billings, MT 800.735.4489 • Casper, WY 886.235.0515 <br />r www.energylab.corn College Station. TX 888.690 2218 • Gillette, WY 866.686.7175 • Helena, MT 877.472.0711 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation <br />Project: Schwartz - SW 5/1/15 S27880, S27882 <br />Analyte Count Result Units <br />Method: E200.7 <br />Report Date: 06/02/15 <br />Work Order: C15050078 <br />RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Analytical Run: ICP4-C_150507A <br />Lab ID: ICV <br />6 Initial Calibration Verification Standard <br />Lab ID: MB -44586 <br />5 Method Blank <br />05/07/15 13:21 <br />Aluminum <br />4.92 mg/L <br />0.10 <br />98 <br />95 <br />105 <br />Boron <br />0.984 mg/L <br />0.050 <br />98 <br />95 <br />105 <br />Iron <br />5.03 mg/L <br />0.030 <br />101 <br />95 <br />105 <br />Manganese <br />4.85 mg/L <br />0.010 <br />97 <br />95 <br />105 <br />Potassium <br />51.3 mg/L <br />1.0 <br />103 <br />95 <br />105 <br />Zinc <br />0.953 mg/L <br />0.010 <br />95 <br />95 <br />105 <br />Lab ID: ICSA <br />6 Interference Check Sample A <br />05/07/15 13:40 <br />Aluminum <br />465 mg/L <br />0.10 <br />93 <br />80 <br />120 <br />Boron <br />0.0136 mg/L <br />0.050 <br />Iron <br />178 mg/L <br />0.030 <br />89 <br />80 <br />120 <br />Manganese <br />-0.0188 mg/L <br />0.010 <br />Potassium <br />-0.00319 mg/L <br />1.0 <br />Zinc <br />-0.00416 mg/L <br />0.010 <br />Lab ID: ICSAB <br />6 Interference Check Sample AB <br />05/07/15 13:44 <br />Aluminum <br />474 mg/L <br />0.10 <br />95 <br />80 <br />120 <br />Boron <br />0.0107 mg/L <br />0.050 <br />Iron <br />181 mg/L <br />0.030 <br />90 <br />80 <br />120 <br />Manganese <br />0.429 mg/L <br />0.010 <br />86 <br />80 <br />120 <br />Potassium <br />-0.00534 mg/L <br />1.0 <br />Zinc <br />0.922 mg/L <br />0.010 <br />92 <br />80 <br />120 <br />Method: E200.7 <br />Lab ID: MB -44586 <br />5 Method Blank <br />Aluminum <br />ND mg/L <br />Boron <br />ND mg/L <br />Iron <br />ND mg/L <br />Manganese <br />ND mg/L <br />Zinc <br />ND mg/L <br />Lab ID: LCS3-44586 <br />5 Laboratory Control Sample <br />Aluminum <br />5.18 mg/L <br />Boron <br />1.00 mg/L <br />Iron <br />5.14 mg/L <br />Manganese <br />4.95 mg/L <br />Zinc <br />0.978 mg/L <br />Lab ID: C15050100-005BMS3 <br />5 Sample Matrix Spike <br />Aluminum <br />5.59 mg/L <br />Boron <br />1.32 mg/L <br />Iron <br />5.41 mg/L <br />Manganese <br />5.18 mg/L <br />Zinc <br />1.03 mg/L <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />Run: ICP4-C 150507A <br />0.02 <br />0.007 <br />0.005 <br />0.001 <br />0.004 <br />ND - Not detected at the reporting limit. <br />Batch: 44586 <br />05/07/15 23:11 <br />05/07/15 23:15 <br />05/08/15 00:26 <br />Page 11 of 31 <br />Run: ICP4-C_150507A <br />0.030 <br />104 <br />85 115 <br />0.050 <br />100 <br />85 115 <br />0.030 <br />103 <br />85 115 <br />0.0012 <br />99 <br />85 115 <br />0.010 <br />98 <br />85 115 <br />Run: ICP4-C_150507A <br />0.15 <br />112 <br />70 130 <br />0.067 <br />103 <br />70 130 <br />0.049 <br />105 <br />70 130 <br />0.012 <br />103 <br />70 130 <br />0.055 <br />103 <br />70 130 <br />ND - Not detected at the reporting limit. <br />Batch: 44586 <br />05/07/15 23:11 <br />05/07/15 23:15 <br />05/08/15 00:26 <br />Page 11 of 31 <br />