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Lab Numbers: 20150129701 - 20150129702 <br />QC Smp <br />Parameter Lab# Value Value Spike DF Result Limits Method <br />Page 2 <br />Initial Calibration Verification <br />Arsenic - D <br />0.050 <br />0.050 <br />1 <br />0.500% <br />(-12.88) - (8.895) <br />EPA 200.8 <br />Barium - D <br />0.052 <br />0.050 <br />1 <br />3.26% <br />(-8.248) - (5.866) <br />EPA 200.8 <br />Cadmium - D <br />0.052 <br />0.050 <br />1 <br />4.48% <br />(-8.841) - (6.851) <br />EPA 200.8 <br />Chromium - D <br />0.050 <br />0.050 <br />1 <br />-0.120% <br />(-8.012) - (7.252) <br />EPA 200.8 DRC <br />Lead - D <br />0.054 <br />0.050 <br />1 <br />7.90% <br />(-8.479) - (9.555) <br />EPA 200.8 <br />Selenium - D <br />0.254 <br />0.250 <br />1 <br />1.54% <br />(-10.71) - (8.927) <br />EPA 200.8 <br />Silver - D <br />0.052 <br />0.050 <br />1 <br />3.94% <br />(-6.551) - (10.28) <br />EPA 200.8 <br />Mercury - T <br />0.0030 <br />0.0030 <br />1 <br />0.333% <br />(-12.61) - (13.11) <br />EPA 245.1 <br />Mercury - T <br />0.0032 <br />0.0030 <br />1 <br />6.33% <br />(-12.32) - (10.37) <br />EPA SW846 7471 B <br />Mercury - TCLP <br />0.0032 <br />0.0030 <br />1 <br />6.33% <br />(-13.95) - (8.049) <br />EPA SW846 7471 B <br />Continuina Calibration Verification <br />Arsenic- D <br />0.045 <br />0.050 <br />1 <br />-9.92% <br />(-13.20) - (5.294) <br />EPA 200.8 <br />Arsenic - D <br />0.053 <br />0.050 <br />1 <br />5.86% <br />(-13.20) - (5.294) <br />EPA 200.8 X <br />Arsenic - D <br />0.047 <br />0.050 <br />1 <br />-6.22% <br />(-13.20) - (5.294) <br />EPA 200.8 <br />Arsenic - D <br />0.046 <br />0.050 <br />1 <br />-8.20% <br />(-13.20) - (5.294) <br />EPA 200.8 <br />Barium - D <br />0.048 <br />0.050 <br />1 <br />-4.18% <br />(-10.54) - (2.945) <br />EPA 200.8 <br />Barium - D <br />0.047 <br />0.050 <br />1 <br />-5.80% <br />(-10.54) - (2.945) <br />EPA 200.8 <br />Barium - D <br />0.046 <br />0.050 <br />1 <br />-7.84% <br />(-10.54) - (2.945) <br />EPA 200.8 <br />Barium - D <br />0.050 <br />0.050 <br />1 <br />0.560% <br />(-10.54) - (2.945) <br />EPA 200.8 <br />Cadmium - D <br />0.046 <br />0.050 <br />1 <br />-7.90% <br />(-14.15) - (6.896) <br />EPA 200.8 <br />Cadmium - D <br />0.047 <br />0.050 <br />1 <br />-6.06% <br />(-14.15) - (6.896) <br />EPA 200.8 <br />Cadmium - D <br />0.045 <br />0.050 <br />1 <br />-9.88% <br />(-14.15) - (6.896) <br />EPA 200.8 <br />Cadmium - D <br />0.052 <br />0.050 <br />1 <br />3.68% <br />(-14.15) - (6.896) <br />EPA 200.8 <br />Chromium - D <br />0.046 <br />0.050 <br />1 <br />-9.10% <br />(-15.69) - (4.513) <br />EPA 200.8 DRC <br />Chromium - D <br />0.049 <br />0.050 <br />1 <br />-2.50% <br />(-15.69) - (4.513) <br />EPA 200.8 DRC <br />Chromium - D <br />0.046 <br />0.050 <br />1 <br />-8.40% <br />(-15.69) - (4.513) <br />EPA 200.8 DRC <br />Lead - D <br />0.048 <br />0.050 <br />1 <br />-3.36% <br />(-11.54) - (10.50) <br />EPA 200.8 <br />Lead - D <br />0.047 <br />0.050 <br />1 <br />-6.64% <br />(-11.54) - (10.50) <br />EPA 200.8 <br />Lead - D <br />0.049 <br />0.050 <br />1 <br />-2.36% <br />(-11.54) - (10.50) <br />EPA 200.8 <br />Lead - D <br />0.054 <br />0.050 <br />1 <br />7.48% <br />(-11.54) - (10.50) <br />EPA 200.8 <br />Selenium - D <br />0.265 <br />0.250 <br />1 <br />6.05% <br />(-12.92) - (5.395) <br />EPA 200.8 X <br />Selenium - D <br />0.233 <br />0.250 <br />1 <br />-6.70% <br />(-12.92) - (5.395) <br />EPA 200.8 <br />Selenium - D <br />0.235 <br />0.250 <br />1 <br />-6.19% <br />(-12.92) - (5.395) <br />EPA 200.8 <br />Selenium - D <br />0.230 <br />0.250 <br />1 <br />-7.99% <br />(-12.92) - (5.395) <br />EPA 200.8 <br />Silver- D <br />0.052 <br />0.050 <br />1 <br />3.72% <br />(-12.07) - (4.911) <br />EPA 200.8 <br />Silver- D <br />0.046 <br />0.050 <br />1 <br />-7.56% <br />(-12.07) - (4.911) <br />EPA 200.8 <br />Silver - D <br />0.048 <br />0.050 <br />1 <br />-3.58% <br />(-12.07) - (4.911) <br />EPA 200.8 <br />Silver - D <br />0.047 <br />0.050 <br />1 <br />-6.36% <br />(-12.07) - (4.911) <br />EPA 200.8 <br />Mercury - T <br />0.0050 <br />0.0050 <br />1 <br />-0.200% <br />(-12.02) - (8.348) <br />EPA 245.1 <br />Mercury - T <br />0.0019 <br />0.0020 <br />1 <br />-6.00% <br />(-12.02) - (8.348) <br />EPA 245.1 <br />Mercury - T <br />0.0010 <br />0.0010 <br />1 <br />-5.00% <br />(-12.02) - (8.348) <br />EPA 245.1 <br />Mercury - T <br />0.0051 <br />0.0050 <br />1 <br />1.60% <br />(-13.97) - (6.378) <br />EPA SW846 7471 B <br />Mercury - T <br />0.0010 <br />0.0010 <br />1 <br />-2.00% <br />(-13.97) - (6.378) <br />EPA SW846 74716 <br />Mercury - T <br />0.0018 <br />0.0020 <br />1 <br />-8.00% <br />(-13.97) - (6.378) <br />EPA SW846 7471 B <br />Mercury - TCLP <br />0.0010 <br />0.0010 <br />1 <br />-2.00% <br />(-12.22) - (5.643) <br />EPA SW846 7471 B <br />