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Lab Numbers: 20150630720-20150630740 Page 3 <br />Initial Calibration Verification <br />Arsenic - D <br />0.050 <br />QC <br />Smp <br />0.840 <br />(-12.44) - (3.566) <br />EPA 200.8 <br />Arsenic - D <br />Parameter <br />Lab# <br />Value <br />Value <br />Spike DF <br />Result <br />Limits <br />Method <br />Matrix Spike Duplicate <br />1 <br />-1.84% <br />(-12.42) - (6.764) <br />EPA 200.8 <br />Barium - D <br />0.048 <br />Selenium - D <br />0806206 <br />11.6 <br />11.7 <br />100 <br />-0.829% <br />(-6.148) - (6.551) <br />EPA 200.8 <br />Selenium - D <br />0807210 <br />1.19 <br />1.17 <br />10 <br />1.43% <br />(-6.148) - (6.551) <br />EPA 200.8 <br />Silver - D <br />0706201 <br />0.226 <br />0.235 <br />10 <br />-4.14% <br />(-6.232) - (3.835) <br />EPA 200.8 <br />Silver - D <br />0807210 <br />2.21 <br />2.25 <br />100 <br />-1.51% <br />(-5.045) - (3.049) <br />EPA 200.8 <br />Silver - D <br />0807210 <br />0.221 <br />0.219 <br />10 <br />0.773% <br />(-5.045) - (3.049) <br />EPA 200.8 <br />Silver - D <br />0806204 <br />0.230 <br />0.233 <br />10 <br />-1.37% <br />(-5.045) - (3.049) <br />EPA 200.8 <br />Silver - D <br />0806206 <br />2.28 <br />2.24 <br />100 <br />1.99% <br />(-5.045) - (3.049) <br />EPA 200.8 <br />Mercury - T <br />0805106 <br />0.0020 <br />0.0020 <br />1 <br />1.98% <br />(-14.94) - (13.09) <br />EPA 245.1 <br />Arsenic - TR <br />0806208 <br />2.27 <br />2.27 <br />100 <br />0.123% <br />(-10.54) - (7.112) <br />EPA 200.8 <br />Arsenic - TR <br />0806201 <br />0.233 <br />0.236 <br />10 <br />-1.02% <br />(-10.54) - (7.112) <br />EPA 200.8 <br />Barium - TR <br />0806208 <br />2.22 <br />2.24 <br />100 <br />-0.934% <br />(-5.955) - (5.446) <br />EPA 200.8 <br />Barium - TR <br />0806201 <br />0.238 <br />0.248 <br />10 <br />-4.40% <br />(-5.955) - (5.446) <br />EPA 200.8 <br />Cadmium - TR <br />0806201 <br />0.230 <br />0.239 <br />10 <br />-3.98% <br />(-4.474) - (3.717) <br />EPA 200.8 <br />Cadmium - TR <br />0806208 <br />2.40 <br />2.43 <br />100 <br />-1.60% <br />(-4.474) - (3.717) <br />EPA 200.8 <br />Chromium - TR <br />0806208 <br />2.17 <br />2.29 <br />100 <br />-5.66% <br />(-8.390) - (9.719) <br />EPA 200.8 DRC <br />Chromium - TR <br />0806201 <br />0.219 <br />0.234 <br />10 <br />-6.49% <br />(-8.390) - (9.719) <br />EPA 200.8 DRC <br />Lead - TR <br />0806201 <br />0.231 <br />0.238 <br />10 <br />-3.01% <br />(-3.197) - (2.651) <br />EPA 200.8 <br />Lead - TR <br />0806208 <br />2.39 <br />2.37 <br />100 <br />0.994% <br />(-3.197) - (2.651) <br />EPA 200.8 <br />Selenium - TR <br />0806208 <br />11.8 <br />11.7 <br />100 <br />1.06% <br />(-5.470) - (4.334) <br />EPA 200.8 <br />Selenium - TR <br />0806201 <br />1.18 <br />1.23 <br />10 <br />-3.84% <br />(-5.470) - (4.334) <br />EPA 200.8 <br />Silver - TR <br />0806201 <br />0.220 <br />0.229 <br />10 <br />-4.16% <br />(-5.600) - (5.278) <br />EPA 200.8 <br />Silver - TR <br />0806208 <br />2.26 <br />2.27 <br />100 <br />-0.287% <br />(-5.600) - (5.278) <br />EPA 200.8 <br />Mercury - TCLP <br />0731554 <br />0.0021 <br />0.0021 <br />1 <br />-3.36% <br />(-15.12) - (15.68) <br />EPA SW846 7471 B <br />Mercury - MEP <br />0630740 <br />0.0019 <br />0.0020 <br />1 <br />-5.15% <br />EPA SW846 7471 B <br />Initial Calibration Verification <br />Arsenic - D <br />0.050 <br />0.050 <br />1 <br />0.840 <br />(-12.44) - (3.566) <br />EPA 200.8 <br />Arsenic - D <br />0.048 <br />0.050 <br />1 <br />-4.52% <br />(-7.865) - (3.017) <br />EPA 200.8 <br />Barium - D <br />0.049 <br />0.050 <br />1 <br />-1.84% <br />(-12.42) - (6.764) <br />EPA 200.8 <br />Barium - D <br />0.048 <br />0.050 <br />1 <br />-5.06% <br />(-8.985) - (3.525) <br />EPA 200.8 <br />Cadmium - D <br />0.051 <br />0.050 <br />1 <br />1.40% <br />(-9.392) - (3.164) <br />EPA 200.8 <br />Cadmium - D <br />0.048 <br />0.050 <br />1 <br />-3.28% <br />(-6.651) - (4.065) <br />EPA 200.8 <br />Chromium - D <br />0.049 <br />0.050 <br />1 <br />-2.02% <br />(-13.46) - (7.323) <br />EPA 200.8 DRC <br />Chromium - D <br />0.053 <br />0.050 <br />1 <br />4.98% <br />(-12.64) - (11.06) <br />EPA 200.8 DRC <br />Lead - D <br />0.051 <br />0.050 <br />1 <br />1.02% <br />(-9.254) - (5.098) <br />EPA 200.8 <br />Lead - D <br />0.051 <br />0.050 <br />1 <br />1.60% <br />(-12.06) - (13.25) <br />EPA 200.8 <br />Selenium - D <br />0.256 <br />0.250 <br />1 <br />2.34% <br />(-7.537) - (4.607) <br />EPA 200.8 <br />Selenium - D <br />0.243 <br />0.250 <br />1 <br />-2.73% <br />(-5.964) - (4.330) <br />EPA 200.8 <br />Silver - D <br />0.051 <br />0.050 <br />1 <br />1.44% <br />(-8.035) - (3.953) <br />EPA 200.8 <br />Silver - D <br />0.048 <br />0.050 <br />1 <br />-3.22% <br />(-7.516) - (6.476) <br />EPA 200.8 <br />Mercury - T <br />0.0031 <br />0.0030 <br />1 <br />2.33% <br />(-10.74) - (6.872) <br />EPA 245.1 <br />Mercury - MEP <br />0.0029 <br />0.0030 <br />1 <br />-3.67% <br />EPA SW846 7471 B <br />Continuing Calibration Verification <br />Arsenic - D <br />0.052 <br />0.050 <br />1 <br />3.16% <br />(-11.63) - (-0.6819) <br />EPA 200.8 X <br />- Recovery <br />was within 10% of expected value <br />