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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Rio Grande Silver, Inc. <br />Project ID: BO 33504 <br />Sample ID: W -B -ALT <br />Zinc, total recoverable <br />M200.8 ICP -MS 1 <br />Wet Chemistry <br />0613011511:10 <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />Bicarbonate as <br />1 <br />CaCO3 <br />mg/L <br />Carbonate as CaCO3 <br />1 <br />Hydroxide as CaCO3 <br />1 <br />Total Alkalinity <br />1 <br />Carbon, dissolved <br />SM5310B 1 <br />organic (DOC) <br />07/02/15 0:00 <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />mg/L <br />Sum of Anions <br />20 <br />Sum of Cations <br />tms <br />Chemical Oxygen <br />M410.4 1 <br />Demand <br />1 <br />Chloride <br />M300.0 - Ion Chromatography 1 <br />Fluoride <br />SM450OF-C 1 <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />Nitrate as N, dissolved <br />Calculation: NO3NO2 minus NO2 <br />Nitrate/Nitrite as N, <br />M353.2 - Automated 1 <br />dissolved <br />Cadmium Reduction <br />Nitrite as N, dissolved <br />M353.2 - Automated 1 <br />Cadmium Reduction <br />Nitrogen, ammonia <br />M350.1 1 <br />Nitrogen, organic <br />M351.2 & M350.1 - TKN minus NH3 <br />Nitrogen, total Kjeldahl <br />M351.2-TKN by Block Digester 1 <br />pH (lab) <br />SM4500H+8 <br />pH <br />1 <br />pH measured at <br />1 <br />Phosphorus, total <br />M365.1 - Auto Ascorbic 1 <br />enb <br />Acid (digest) <br />Residue, Filterable <br />SM2540C 1 <br />(TDS) @180C <br />2.5 <br />Residue, Non- <br />SM2540D 1 <br />Filterable (TSS) <br />B <br />@105C <br />0.05 <br />Sulfate <br />M300.0 - Ion Chromatography 1 <br />Sulfide as S <br />SM450oS2-D 1 <br />REPIN.02.06.05.01 <br />L25209-1507241357 <br />ACZ Sample ID: <br />L25209-02 <br />Date Sampled: <br />0613011511:10 <br />Date Received: <br />07/01/15 <br />Sample Matrix: <br />Surface Water <br />0.690 mg/L 0.002 0.005 07/09/1514:00 scp <br />21.2 <br />mg/L <br />2 <br />20 <br />07/02/15 0:00 <br />tms <br />U <br />mg/L <br />2 <br />20 <br />07/02/15 0:00 <br />tms <br />U <br />mg/L <br />2 <br />20 <br />07/02/15 0:00 <br />tms <br />21.2 <br />mg/L <br />2 <br />20 <br />07/02/15 0:00 <br />tms <br />U " <br />mg/L <br />1 <br />5 <br />07/23/1515:33 <br />jlf <br />-0.5 <br />% <br />07/24/1511:19 <br />calc <br />0.723 <br />meq/L <br />07/24/1511:19 <br />calc <br />0.716 <br />meq/L <br />07/24/1511:19 <br />calc <br />U <br />mg/L <br />10 <br />20 <br />07/06/1516:00 <br />enb <br />U " <br />mg/L <br />0.5 <br />2.5 <br />07/10/15 2:49 <br />bsu <br />0.06 <br />B <br />mg/L <br />0.05 <br />0.3 <br />07/08/1513:15 <br />enb <br />27 <br />mg/L <br />0.8 <br />4 <br />07/24/1511:19 <br />calc <br />0.21 <br />mg/L <br />0.02 <br />0.1 <br />07/24/1511:19 <br />calc <br />0.21 <br />mg/L <br />0.02 <br />0.1 <br />07/01/1517:18 <br />jlf <br />U <br />mg/L <br />0.01 <br />0.05 <br />07/01/1517:18 <br />jlf <br />U <br />mg/L <br />0.05 <br />0.2 <br />07/13/1513:47 <br />jlf <br />0.1 <br />B <br />mg/L <br />0.1 <br />0.5 <br />07/24/1511:19 <br />calc <br />0.1 <br />B * <br />mg/L <br />0.1 <br />0.5 <br />07/09/15 23:20 <br />pjb <br />7.8 <br />H <br />units <br />0.1 <br />0.1 <br />07/02/15 0:00 <br />tms <br />20.5 <br />C <br />0.1 <br />0.1 <br />07/02/15 0:00 <br />tms <br />0.05 <br />mg/L <br />0.01 <br />0.05 <br />07/10/15 20:56 <br />pjb <br />50 <br />mg/L <br />10 <br />20 <br />07/01/1515:15 <br />enb <br />5.0 <br />B <br />mg/L <br />5 <br />20 <br />07/02/1515:42 <br />enb <br />13.4 <br />mg/L <br />0.5 <br />2.5 <br />07/10/15 2:49 <br />bsu <br />U <br />mg/L <br />0.02 <br />0.1 <br />07/06/1515:21 <br />enb <br />* Please refer to Qualifier Reports for details. <br />Page 8 of 45 <br />