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PIVL Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sennas. CO 80487 (800) 334-5493 <br />Aspen Industrial, Inc ACZ Sample ID: L19808-02 <br />Project ID. Date Sampled: 08105/14 14:00 <br />Sample ID: LUCKY STRIKE MILL UPPER Date Received: 08106/14 <br />Sample Matrix: Surface Water <br />Wet Chemistry <br />Parameter <br />EPA Method Dilution <br />Result <br />Qual XQ <br />Units <br />MDLPQL <br />Date Analyst <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />Bicarbonate as <br />1 <br />157 <br />mg/L <br />2 <br />20 <br />08/07/14 0:00 <br />id <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />9.5 <br />B <br />mg/L <br />2 <br />20 <br />08/07/14 0:00 <br />id <br />Hydroxide as CaCC3 <br />1 <br />U <br />mg/L <br />2 <br />20 <br />08/07/14 0:00 <br />id <br />Total Alkalinity <br />1 <br />166 <br />mg/L <br />2 <br />20 <br />08/07/14 0:00 <br />id <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />0.0 <br />% <br />08/20/14 9:01 <br />Calc <br />Sum of Anions <br />12 <br />meq/L <br />08/20/14 9:01 <br />talc <br />Sum of Cations <br />12 <br />meq/L <br />08/20/14 9:01 <br />talc <br />Chloride <br />SM4500CI-E <br />1 <br />55.7 <br />mg/L <br />0.5 <br />2 <br />08/12/1415:50 <br />bsu <br />Conductivity @25C <br />SM2510B <br />1 <br />1280 <br />umhos/cm <br />1 <br />10 <br />08/07/14 18:27 <br />id <br />Cyanide, total <br />M335.4 - Colonmetnc w/ distillation <br />0.5 <br />U * <br />mg/L <br />0.003 <br />0.01 <br />08/15/14 11:29 <br />mss2 <br />Hardness as CaCO3 <br />SM23408. Calculation <br />106 <br />mg/L <br />0.8 <br />4 <br />08/20/14 9:01 <br />Calc <br />Lab Filtration (0.45um <br />SOPwCo50 <br />1 <br />08/11/14 9:29 <br />djc <br />filter) <br />Lab Filtration (0.45um) <br />M200.7r200.8 <br />1 <br />08/08/14 13:25 <br />mfm <br />& Acidification <br />Nitrate as N, dissolved <br />Calculation: NO3NO2 minus NO2 <br />6.9 <br />mg/L <br />0.1 <br />0.5 <br />08/20/14 9:01 <br />Calc <br />Nitrate/Nitrite as N, <br />M353.2 - Automated <br />5 <br />7.4 <br />mg/L <br />0.1 <br />0.5 <br />08/06/14 23:37 <br />pib <br />dissolved <br />Cadmium Reduction <br />Nitrite as N, dissolved <br />M353.2 - Automated <br />1 <br />0.54 <br />* <br />mg/L <br />0.01 <br />0.05 <br />08/06/14 23:17 <br />pib <br />Cadmium Reduction <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.4 <br />H <br />units <br />0.1 <br />0.1 <br />08/07/14 0:00 <br />id <br />pH measured at <br />1 <br />19.9 <br />C <br />0.1 <br />0.1 <br />08/07/14 0:00 <br />id <br />Residue, Filterable <br />SM2540C <br />1 <br />940 <br />mg/L <br />10 <br />20 <br />08/06/14 16:09 <br />djc <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />178 <br />* <br />mg/L <br />5 <br />20 <br />08/07/14 11:34 <br />nml <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516-02/-07 - Turbidimetric <br />50 <br />306 <br />mg/L <br />50 <br />250 <br />08/13/14 15:13 <br />jlf <br />TDS (calculated) <br />Calculation <br />773 <br />mg/L <br />08/20/14 9:01 <br />Calc <br />TDS (ratio - <br />Calculation <br />1.22 <br />08/20/14 9:01 <br />talc <br />measured/calculated) <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />L19808-1408201022 Page 5 of 26 <br />