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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Gold Hill Mines, Inc. ACZ Project ID: L23406 <br />METHODACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br />L23406-01 WG380998 Manganese, dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG380931 Residue, Filterable (TDS) @180C SM2540C Q6 Sample was received above recommended temperature. <br />WG381394 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />D516-02/-07 - Turbidimetric Q6 Sample was received above recommended temperature. <br />L23406-02 WG380998 Manganese, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG380931 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG381394 Sulfate <br />D516-02/-07 - Turbidimetric <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />D516-02/-07 - Turbidimetric <br />Q6 <br />Sample was received above recommended temperature. <br />L23406-03 WG380998 Manganese, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG380931 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG381394 Sulfate <br />D516-02/-07 - Turbidimetric <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />D516-02/-07 - Turbidimetric <br />Q6 <br />Sample was received above recommended temperature. <br />L23406-04 WG381029 Manganese, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG380931 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG381394 Sulfate <br />D516-02/-07 - Turbidimetric <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />D516-02/-07 - Turbidimetric <br />Q6 <br />Sample was received above recommended temperature. <br />REPAD.15.06.05.01 <br />L23406-1504031101 Page 9 of 12 <br />