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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Gold Hill Mines, Inc. ACZ Project ID: L22296 <br />METHODACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br />L22296-01 WG377287 Zinc, dissolved M200.8 ICP -MS M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG377180 Residue, Filterable (TDS) @180C SM2540C H3 Sample was received and analyzed past holding time. <br />WG377276 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />L22296-02 WG377287 Zinc, dissolved M200.8 ICP -MS M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG377165 Residue, Filterable (TDS) @180C SM2540C H3 Sample was received and analyzed past holding time. <br />WG377276 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />L22296-03 WG377287 Zinc, dissolved M200.8 ICP -MS M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG377165 Residue, Filterable (TDS) @180C SM2540C H3 Sample was received and analyzed past holding time. <br />WG377276 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />L22296-04 WG377287 Zinc, dissolved M200.8 ICP -MS M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG377165 Residue, Filterable (TDS) @180C SM2540C H3 Sample was received and analyzed past holding time. <br />WG377276 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />L22296-05 WG377287 Zinc, dissolved M200.8 ICP -MS M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG377165 Residue, Filterable (TDS) @180C SM2540C H3 Sample was received and analyzed past holding time. <br />WG377276 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />L22296-06 WG377287 Zinc, dissolved M200.8 ICP -MS M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG377165 Residue, Filterable (TDS) @180C SM2540C H3 Sample was received and analyzed past holding time. <br />WG377276 Sulfate D516-02/-07 - Turbidimetric M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />REPAD.15.06.05.01 <br />L22296-1501191306 Page 10 of 14 <br />