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A CZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Gold Hill Mines, Inc. ACZ Project ID: L149O2 <br />ID WOAkNUM PARAMETER <br />METHOD'ACZ <br />dUAL <br />DESCRIPTION <br />L14902-01 WG353021 Manganese, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />Zinc, dissolved <br />M200.7 ICP <br />M3 <br />or LFB) was acceptable. <br />Zinc, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />WG352624 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />or LFB) was acceptable. <br />WG352624 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG353136 Sulfate <br />D516-02 - Turbidimetric <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />D516-02 - Turbidimetric <br />Q6 <br />or LFB) was acceptable. <br />D516-02 - Turbidimetric <br />Q6 <br />Sample was received above recommended temperature. <br />D516-02 - Turbidimetric <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />D516-02 - Turbidimetric <br />ZU <br />accurate evaluation (< 10x MDL). <br />D516-02 - Turbidimetric <br />ZU <br />Analysis date/time preceeds filter date/time. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />L14902-02 WG353021 Manganese, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Zinc, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG352624 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG353136 Sulfate <br />D516-02 - Turbidimetric <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />D516-02 - Turbidimetric <br />Q6 <br />Sample was received above recommended temperature. <br />D516-02 - Turbidimetric <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />D516-02 - Turbidimetric <br />ZU <br />Analysis date/time preceeds filter date/time. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />L14902-03 WG353021 Manganese, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />Zinc, dissolved <br />M200.7 ICP <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />WG352624 Residue, Filterable (TDS) @180C <br />SM2540C <br />Q6 <br />Sample was received above recommended temperature. <br />WG353136 Sulfate <br />D516-02 - Turbidimetric <br />M3 <br />The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />D516-02 - Turbidimetric <br />Q6 <br />Sample was received above recommended temperature. <br />D516-02 - Turbidimetric <br />RA <br />Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />D516-02 - Turbidimetric <br />ZU <br />Analysis date/time preceeds filter date/time. A portion of <br />sample was filtered and analyzed prior to the creation of a <br />Filter workgroup. <br />REPAD.15.06.05.01 <br />Page 14 of 18 <br />