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ACZ Laboratories, Inc. <br />New Elk Mine <br />ACZ Sample ID: <br />L16810 -01 <br />Project ID: <br />Date Sampled: <br />02112114 11:30 <br />Sample ID: PAW -1 <br />Date Received: <br />02113114 <br />Sample Matrix: <br />Ground Water <br />Wet Chemistry <br />Parameter <br />EPA Method Dilution <br />Result <br />Qual <br />XQ Units <br />MDL <br />PQL <br />Date Analyst <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />Bicarbonate as <br />1 <br />169 <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />3 <br />B <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Hydroxide as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Total Alkalinity <br />1 <br />173 <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />-3.7 <br />% <br />02/27/14 16:13 <br />calc <br />Sum of Anions <br />4.2 <br />meq /L <br />0.1 <br />0.5 <br />02/27/14 16:13 <br />calc <br />Sum of Cations <br />3.9 <br />meq /L <br />0.1 <br />0.5 <br />02/27/14 16:13 <br />calc <br />Chloride <br />SM4500CI -E <br />1 <br />7 <br />* mg /L <br />1 <br />5 <br />02/26/1411:50 <br />bsu <br />Conductivity @25C <br />SM2510B <br />1 <br />380 <br />umhos /cm <br />1 <br />10 <br />02/17/14 18:35 <br />abd <br />Fluoride <br />SM450OF -C <br />1 <br />0.3 <br />B <br />* mg /L <br />0.1 <br />0.5 <br />02/25/1412:02 <br />abd <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />154 <br />mg /L <br />1 <br />7 <br />02/27/14 16:13 <br />calc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />02/25/14 10:15 <br />abd <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />02/17/14 15:33 <br />mfm <br />& Acidification <br />Nitrate as N, dissolved <br />Calculation: NO3NO2 minus NO2 <br />U <br />mg /L <br />0.02 <br />0.1 <br />02/27/14 16:13 <br />calc <br />Nitrate /Nitrite as N, <br />M353.2 - Automated <br />1 <br />U <br />mg /L <br />0.02 <br />0.1 <br />02/13/14 20:55 <br />pjb <br />dissolved <br />Cadmium Reduction <br />Nitrite as N, dissolved <br />M353.2 - Automated <br />1 <br />U <br />* mg /L <br />0.01 <br />0.05 <br />02/13/14 20:55 <br />pjb <br />Cadmium Reduction <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.3 <br />H <br />units <br />0.1 <br />0.1 <br />02/17/14 0:00 <br />abd <br />pH measured at <br />1 <br />21 <br />C <br />0.1 <br />0.1 <br />02/17/14 0:00 <br />abd <br />Residue, Filterable <br />SM2540C <br />1 <br />220 <br />mg /L <br />10 <br />20 <br />02/18/14 16:07 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />29 <br />mg /L <br />5 <br />20 <br />02/19/14 11:26 <br />abd <br />Filterable (TSS) <br />@105C <br />Sodium Adsorption <br />USGS - 11738 -78 <br />0.63 <br />0.03 <br />0.15 <br />02/27/14 16:13 <br />calc <br />Ratio in Water <br />Sulfate <br />D516 -02 - Turbidimetric <br />1 <br />25.0 <br />mg /L <br />1 <br />5 <br />02/26/14 16:03 <br />bsu <br />TDS (calculated) <br />Calculation <br />209 <br />mg /L <br />10 <br />50 <br />02/27/14 16:13 <br />calc <br />TDS (ratio - <br />Calculation <br />1.05 <br />02/27/14 16:13 <br />calc <br />measured /calculated) <br />Arizona license number: AZO102 <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />L16810- 1402281024 Page 3 of 30 <br />