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AC Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Aspen Industrial, Inc ACZ Project ID: L19808 <br />L19808 -01 WG369476 Cadmium, dissolved M200.8 ICP -MS <br />WG369506 Cyanide, total M335.4 - Colorimetric wl <br />distillation <br />WG369038 Nitrate /Nitrite as N, dissolved M353.2 - Automated Cadmium <br />Reduction <br />Nitrite as N, dissolved M353.2 - Automated Cadmium <br />Reduction <br />WG369378 Sulfate D516 -02/ -07 - Turbidimetric <br />L19808 -02 WG369099 Aluminum, total M200.7 ICP <br />Iron, total M200.7 ICP <br />WG369506 <br />Cyanide, total <br />M335.4 - Colorimetric w/ <br />distillation <br />WG369038 <br />Nitrate/Nitrite as N, dissolved <br />M353.2 - Automated Cadmium <br />Reduction <br />Nitrite as N, dissolved <br />M353.2 - Automated Cadmium <br />Reduction <br />WG369068 <br />Residue, Non - Filterable (TSS) @105C <br />SM2540D <br />WG369378 <br />Sulfate <br />D516 -02/ -07 - Turbidimetric <br />L19808 -03 WG369099 Aluminum, total <br />Iron, total <br />WG369506 Cyanide, total <br />WG369038 Nitrate /Nitrite as N, dissolved <br />Nitrite as N, dissolved <br />M200.7 ICP <br />M200.7 ICP <br />M335.4 - Colorimetric w/ <br />distillation <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />WG369068 Residue, Non - Filterable (TSS) @105C SM2540D <br />WG369378 Sulfate D516 -02/ -07 - Turbidimetric <br />REPAD.15.06.05.01 <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 1 Ox MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />L19808- 1408201022 Page 21 of 26 <br />