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ADZ Laboratories, Inc. <br />Aspen Industrial, Inc ACZ Project ID: L19808 <br />Copper, dissolved <br />WG369188 <br />WG3691881CV <br />WG369188ICB <br />WG369188LFB <br />L 19808 -01 AS <br />L19808 -01 ASD <br />Copper, total <br />WG369099 <br />M200.7 ICP <br />ICV <br />08/11/1415:19 <br />11140729 -1 <br />2 <br />1.971 <br />mg /L <br />98.6 <br />95 <br />105 <br />ICB <br />08/11/1415:25 <br />ICV <br />WG369099ICB <br />U <br />mg /L <br />1.984 <br />-0.03 <br />0.03 <br />LFB <br />08/11/1415:38 <br />11140808 -3 <br />.4995 <br />.503 <br />mg /L <br />100.7 <br />85 <br />115 <br />AS <br />08/11/1416:00 <br />11140808 -3 <br />.4995 <br />U .512 <br />mg /L <br />102.5 <br />85 <br />115 <br />ASD <br />08/11/1416:03 <br />11140808 -3 <br />.4995 <br />U .512 <br />mg /L <br />102.5 <br />85 <br />115 0 20 <br />M200.7 ICP <br />WG3690991CV <br />ICV <br />08/08/1410:52 <br />11140730 -3 <br />2 <br />1.996 <br />mg /L <br />99.8 <br />95 <br />105 <br />ICV <br />WG369099ICB <br />ICB <br />08/08/1410:58 <br />1.984 <br />mg /L <br />99.2 <br />U <br />mg /L <br />WG369099ICB <br />-0.03 <br />0.03 <br />WG369082LRB <br />LRB <br />08/08/1411:10 <br />-0.06 <br />0.06 <br />U <br />mg /L <br />08/08/1411:10 <br />-0.022 <br />0.022 <br />U <br />WG369082LFB <br />LFB <br />08/08/1411:14 <br />11140722 -2 <br />.4995 <br />LFB <br />.491 <br />mg /L <br />98.3 <br />85 <br />115 <br />100.3 <br />L19808 -02LFM <br />LFM <br />08/08/1411:48 <br />11140722 -2 <br />.4995 <br />.01 <br />.501 <br />mg /L <br />98.3 <br />70 <br />130 <br />130 M3 <br />L19808- 02LFMD <br />LFMD <br />08/08/1411:51 <br />11140722 -2 <br />.4995 <br />.01 <br />.503 <br />mg /L <br />98.7 <br />70 <br />130 <br />0.4 20 <br />Cyanide, total <br />ACZ ID <br />Type <br />Analyzed <br />M335.4 - Colorimetric w/ distillation <br />PCN/SCN w <br />WG369506 <br />WG3695061CV <br />ICV <br />08/15/1411:22 <br />W1140801 -6 <br />.3 <br />.2791 <br />mg /L <br />93 <br />90 <br />110 <br />WG3695061CB <br />ICB <br />08/15/1411:23 <br />U <br />mg /L <br />-0.003 <br />0.003 <br />WG369348LRB <br />LRB <br />08/15/1411:24 <br />U <br />mg /L <br />-0.003 <br />0.003 <br />WG369348LFB <br />LFB <br />08/15/1411:24 <br />W1140801 -2 <br />.2 <br />.2028 <br />mg /L <br />101.4 <br />90 <br />110 <br />L19779 -04DUP <br />DUP <br />08/15/1411:26 <br />U <br />U <br />mg /L <br />0 20 RA <br />L19808 -01LFM <br />LFM <br />08/15/1411:28 <br />W1140801 -2 <br />.2 <br />U <br />.1912 <br />mg /L <br />95.6 <br />90 <br />110 <br />Iron, dissolved <br />ACZ ID <br />Type <br />Analyzed <br />M200.7 ICP <br />PCNiSCN <br />Qc <br />Sample <br />Found <br />Units <br />Rec <br />Lower <br />Upper <br />RPD Limit Qual <br />WG369188 <br />WG3691881CV <br />ICV <br />08/11/1415:19 <br />11140729 -1 <br />2 <br />1.98 <br />mg /L <br />99 <br />95 <br />105 <br />WG369188ICB <br />ICB <br />08/11/1415:25 <br />U <br />mg /L <br />-0.06 <br />0.06 <br />WG369188LFB <br />LFB <br />08/11/1415:38 <br />11140808 -3 <br />1.0014 <br />1.045 <br />mg /L <br />104.4 <br />85 <br />115 <br />L19808 -01AS <br />AS <br />08/11/1416:00 <br />11140808 -3 <br />1.0014 <br />.03 <br />1.056 <br />mg /L <br />102.5 <br />85 <br />115 <br />L19808 -01ASD <br />ASD <br />08/11/1416:03 <br />11140808 -3 <br />1.0014 <br />.03 <br />1.054 <br />mg /L <br />102.3 <br />85 <br />115 <br />0.19 20 <br />Iron, total M200.7 ICP <br />W G369099 <br />WG3690991CV <br />ICV <br />08/08/1410:52 <br />11140730 -3 <br />2 <br />1.984 <br />mg /L <br />99.2 <br />95 <br />105 <br />WG369099ICB <br />ICB <br />08/08/1410:58 <br />U <br />mg /L <br />-0.06 <br />0.06 <br />WG369082LRB <br />LRB <br />08/08/1411:10 <br />U <br />mg /L <br />-0.044 <br />0.044 <br />WG369082LFB <br />LFB <br />08/08/1411:14 <br />11140722 -2 <br />1.0014 <br />1.004 <br />mg /L <br />100.3 <br />85 <br />115 <br />L19808 -02LFM <br />LFM <br />08/08/1411:48 <br />11140722 -2 <br />1.0014 <br />9.55 11.01 <br />mg /L <br />145.8 <br />70 <br />130 M3 <br />L19808- 02LFMD <br />LFMD <br />08/08/1411:51 <br />11140722 -2 <br />1.0014 <br />9.55 11.35 <br />mg /L <br />179.7 <br />70 <br />130 3.04 20 M3 <br />L19808- 1408201022 Page 14 of 26 <br />