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A CZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sorinos. CO 80487 /8001 334 -5493 <br />Aspen Industrial, Inc ACZ Project ID: L19808 <br />Arsenic, dissolved <br />ACZ ID Type <br />Analyzed <br />M200.8 ICP -MS <br />PCN/SCN Qc <br />Sample <br />Found <br />Units <br />Rec <br />Lower <br />Upper <br />RPD Limit Qual <br />WG369476 <br />WG3694761CV <br />ICV <br />08/14/14 23:43 <br />MS140723 -1 <br />.05 <br />.05257 <br />mg /L <br />105.1 <br />90 <br />110 <br />WG3694761CB <br />ICB <br />08/14/14 23:46 <br />U <br />mg /L <br />- 0.0006 <br />0.0006 <br />WG369476LFB <br />LFB <br />08/14/14 23:49 <br />MS140728 -3 <br />.0501 <br />.04881 <br />mg /L <br />97.4 <br />85 <br />115 <br />L19791 -05AS <br />AS <br />08/15/14 0:09 <br />MS140728 -3 <br />.2505 <br />U <br />.2409 <br />mg /L <br />96.2 <br />70 <br />130 <br />L19791 -05ASD <br />ASD <br />08/15/14 0:12 <br />MS140728 -3 <br />.2505 <br />U <br />.2362 <br />mg /L <br />94.3 <br />70 <br />130 <br />1.97 20 <br />Arsenic, total <br />ACZ ID <br />Type <br />Analyzed <br />M200.8 ICP -MS <br />PCNISCN oc <br />Sample <br />Found <br />Units <br />Rec <br />Lower <br />Upper <br />RPD Limit Qual <br />WG369551 <br />WG3695511CV <br />ICV <br />08/15/1421:49 <br />MS140723 -1 <br />.05 <br />.05176 <br />mg /L <br />103.5 <br />90 <br />110 <br />WG369551ICB <br />ICB <br />08/15/1421:52 <br />U <br />mg /L <br />- 0.0006 <br />0.0006 <br />WG369321LRB <br />LRB <br />08/15/1421:55 <br />U <br />mg /L <br />- 0.00044 <br />0.00044 <br />WG369321LFB <br />LFB <br />08/15/1421:58 <br />MS140728 -3 <br />.0501 <br />.04925 <br />mg /L <br />98.3 <br />85 <br />115 <br />L19850 -03LFM <br />LFM <br />08/15/14 22:33 <br />MS140728 -3 <br />.0501 <br />.004 <br />.0546 <br />mg /L <br />101 <br />70 <br />130 <br />L19850- 03LFMD <br />LFMD <br />08/15/14 22:36 <br />MS140728 -3 <br />.0501 <br />.004 <br />.0532 <br />mg /L <br />98.2 <br />70 <br />130 <br />2.6 20 <br />Barium, dissolved <br />�ACZ ID Type <br />Analyzed <br />M200.7 ICP <br />PCN/SCN <br />• <br />WG369188 <br />WG3691881CV <br />ICV <br />08/11/1415:19 <br />11140729 -1 <br />2 <br />1.9685 <br />mg /L <br />98.4 <br />95 <br />105 <br />WG369188ICB <br />ICB <br />08/11/1415:25 <br />.004 <br />mg /L <br />-0.009 <br />0.009 <br />WG369188LFB <br />LFB <br />08/11/1415:38 <br />11140808 -3 <br />.5 <br />.5029 <br />mg /L <br />100.6 <br />85 <br />115 <br />L19808 -01AS <br />AS <br />08/11/1416.00 <br />11140808 -3 <br />.5 <br />.217 <br />.7091 <br />mg /L <br />98.4 <br />85 <br />115 <br />L19808 -01ASD <br />ASD <br />08/11/1416:03 <br />11140808 -3 <br />.5 <br />.217 <br />.7099 <br />mg /L <br />98.6 <br />85 <br />115 <br />0.11 20 <br />Barium, total <br />;ACZ ID <br />Type <br />Analyzed <br />M200.7 ICP <br />PCN/SCN <br />w <br />WG369099 <br />WG3690991CV <br />ICV <br />08/08/1410:52 <br />11140730 -3 <br />2 <br />1.9955 <br />mg /L <br />99.8 <br />95 <br />105 <br />WG369099ICB <br />ICB <br />08/08/1410:58 <br />U <br />mg /L <br />-0.009 <br />0.009 <br />WG369082LRB <br />LRB <br />08/08/1411:10 <br />U <br />mg /L <br />- 0.0066 <br />0.0066 <br />WG369082LFB <br />LFB <br />08/08/1411:14 <br />11140722 -2 <br />.5 <br />.4903 <br />mg /L <br />98.1 <br />85 <br />115 <br />L19808 -02LFM <br />LFM <br />08/08/1411:48 <br />11140722 -2 <br />.5 <br />.048 <br />.5418 <br />mg /L <br />98.8 <br />70 <br />130 <br />L19808- 02LFMD <br />LFMD <br />08/08/1411:51 <br />11140722 -2 <br />.5 <br />.048 <br />.5495 <br />mg /L <br />100.3 <br />70 <br />130 <br />1.41 20 <br />Beryllium, dissolved <br />ACZ ID Type <br />Analyzed <br />M200.8 ICP -MS <br />PCN/SCN ac <br />Sample <br />Found <br />Units <br />Rec <br />Lower <br />Upper <br />RPD Limit Qual <br />WG369476 <br />WG3694761CV <br />ICV <br />08/14/1423:43 <br />MS140723 -1 <br />.05 <br />.04637 <br />mg /L <br />92.7 <br />90 <br />110 <br />WG3694761CB <br />ICB <br />08/14/14 23:46 <br />U <br />mg /L <br />- 0.00015 <br />0.00015 <br />WG369476LFB <br />LFB <br />08/14/14 23:49 <br />MS140728 -3 <br />.05005 <br />.0452 <br />mg /L <br />90.3 <br />85 <br />115 <br />L19791 -05AS <br />AS <br />08/15/14 0:09 <br />MS140728 -3 <br />.25025 <br />.0005 <br />.2173 <br />mg /L <br />86.6 <br />70 <br />130 <br />L19791 -05ASD <br />ASD <br />08/15/14 0:12 <br />MS140728 -3 <br />.25025 <br />.0005 <br />.2151 <br />mg /L <br />85.8 <br />70 <br />130 <br />1.02 20 <br />L19808- 1408201022 Page 11 of 26 <br />