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One Government Gulch-PO Box 929 Kellogg ID 83837-0929 (208)784-1258 Fax(208)783-0891 <br /> McClelland Laboratories Inc Project Name:MLI:3819 <br /> 1016 Greg Street Work Order: W4B0077 <br /> Sparks,NV 89431 Reported: 13-Mar-14 15:02 <br /> Quality Control-BLANK Data <br /> Method Analyte Units Result MDL MRL Batch ID Analyzed Notes <br /> Acid/Base Accounting&Sulfur Forms <br /> Modified Sobek ANP TCaCO3/kT <0.3 0.1 0.3 W407027 13-Feb-14 <br /> Modified Sobek Non-extractable % <0.01 0 006 0.01 W407027 14-Feb-14 <br /> Sulfur <br /> Modified Sobek Non-Sulfate Sulfur % <0.01 0.006 0 01 W407027 14-Feb-14 <br /> Modified Sobek Total Sulfur % <0.01 0.006 0.01 W407027 14-Feb-14 <br /> Modified Sobek Total Sulfur % <0.01 0.006 0.01 W407027 17-Feb-14 <br /> Acid/Base Accounting&Sulfur Forms(HCI Wash) <br /> Modified Sobek Non-extractable % <0.01 0.006 0.01 W407027 14-Feb-14 <br /> Sulfur <br /> Modified Sobek Non-Sulfate % <0 01 0.006 0.01 W407027 14-Feb-14 <br /> Sulfur-HCI <br /> Modified Sobek Non-Sulfate % <0.01 0.006 0.01 W407027 17-Feb-14 <br /> Sulfur-HC1 <br /> Modified Sobek Total Sulfur % <0.01 0.006 0.01 W407027 14-Feb-14 <br /> Modified Sobek Total Sulfur % <0.01 0.006 0.01 W407027 17-Feb-14 <br /> Quality Control-LABORATORY CONTROL SAMPLE Data <br /> LCS LCS % Acceptance <br /> Method Analyte Units Result True Rec. Limits Batch ID Analyzed Notes <br /> Acid/Base Accounting&Sulfur Forms <br /> Modified Sobek ANP TCaCO3/kT 212 216 98.0 80-120 W407027 13-Feb-14 <br /> Modified Sobek Total Sulfur % 1.84 2.00 92.0 80-120 W407027 14-Feb-14 <br /> Acid/Base Accounting&Sulfur Forms(HCI Wash) <br /> Modified Sobek Total Sulfur % 1.84 2.00 92.0 80-120 W407027 14-Feb-14 <br /> Classical Chemistry Parameters <br /> EPA 600/2-78-054 Paste pH pH Units 7.31 7.40 98.8 93.7-106.3 W407020 12-Feb-14 <br /> EPA 600/2-78-054 Paste pH pH Units 7.44 7.40 101 93.7-106.3 W411205 13-Mar-14 <br /> Quality Control-DUPLICATE Data <br /> Duplicate Sample RPD <br /> Method Analyte Units Result Result RPD Limit Batch ID Analyzed Notes <br /> Acid/Base Accounting&Sulfur Forms <br /> Modified Sobek ANP TCaCO3/kT 136 136 0.0 20 W407027 13-Feb-14 <br /> Modified Sobek Non-extractable % <0.01 <0.01 UDL 20 W407027 14-Feb-14 <br /> Sulfur <br /> Modified Sobek Non-Sulfate Sulfur % 0.38 0.42 8.5 20 W407027 14-Feb-14 <br /> Modified Sobek Total Sulfur % 0.07 0.06 8.3 20 W407027 17-Feb-14 <br /> Modified Sobek Total Sulfur % 0 74 0.75 2.1 20 W407027 14-Feb-14 <br /> Acid/Base Accounting&Sulfur Forms(HCI Wash) <br /> Modified Sobek Non-extractable % <0 01 <0.01 UDL 20 W407027 14-Feb-14 <br /> Sulfur <br /> Modified Sobek Non-Sulfate % 0.09 0.08 8.9 20 W407027 17-Feb-14 <br /> Sulfur-HCI <br /> Modified Sobek Non-Sulfate % 0 45 0.48 6.7 20 W407027 14-Feb-14 <br /> Sulfa-HCI <br /> Modified Sobek Total Sulfur % 0.07 0.07 4.7 20 W407027 17-Feb-14 <br /> SVL holds the following certifications. <br /> AZ:0538,CA:2080,FL(NELAC):E87993,ID:ID00019&ID00965(Microbiology),NV:ID000192007A,WA:C573 Work order Report Page 3 of 4 <br />