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AUZ Laboratories, Inc. • • • • • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 O - • • <br /> Golder Associates ACZ Project ID: L20231 <br /> METHODACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br /> L20231-01 WG370454 Barium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG370695 Chloride M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> Sulfate M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> L20231-02 WG370454 Barium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG370695 Chloride M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> WG370424 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<1 Ox MDL). <br /> WG370695 Sulfate M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> L20231-03 WG370454 Barium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG370695 Chloride M300.0-Ion Chromatography M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable. <br /> Sulfate M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> L20231-04 WG370493 Manganese,dissolved M200.7 ICP D1 Sample required dilution due to matrix. <br /> WG370695 Chloride M300.0-Ion Chromatography M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable. <br /> WG370345 pH SM4500H+B ZW Method deviation. The sample was centrifuged prior to <br /> analysis due to high solid content. <br /> WG370424 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> WG370695 Sulfate M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> W G370345 Total Alkalinity SM2320B-Titration ZW Method deviation. The sample was centrifuged prior to <br /> analysis due to high solid content. <br /> L20231-05 WG370695 Chloride M300.0-Ion Chromatography M1 Matrix spike recovery was high,the recovery of the <br /> associated control sample(LCS or LFB)was acceptable. <br /> WG370424 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> WG370695 Sulfate M300.0-Ion Chromatography DC Sample required dilution. Non-target analyte exceeded <br /> calibration range. <br /> M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> REPAD.15.06.05.01 <br /> L20231-1409110853 Page 17 of 23 <br />