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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Peabody Sage Creek Mining, LLC <br />Project ID: 451288047 <br />Sample ID: NPDES4 <br />Inorganic Prep <br />ACZ Sample ID: <br />L18137 -01 <br />Date Sampled: <br />05107114 14:50 <br />Date Received: <br />05107114 <br />Sample Matrix: <br />Surface Water <br />;fir,a9– <br />ff Qk-i Z L,ilUk(w..b I �jilL Cko - <br />af i , <br />4ko (ic <br />Acidify and filter <br />_ <br />Colorado 5 CCR 1002- <br />05/08/14 6:55 <br />las <br />(Potentially Dissolved) <br />31.5.31 (2009) <br />- - - -- -- <br />M200.7 ICP <br />1 <br />Total Recoverable <br />M200.2 ICP -MS <br />05/12/14 15:12 <br />[as <br />Digestion <br />jjc <br />Selenium, potentially <br />M200.8 ICP -MS <br />Total Recoverable <br />M200.2 ICP <br />05/12/14 15:02 <br />aeb /jjc <br />Digestion <br />Metals Analysis <br />(TDS) @180C <br />REPIN.02.06.05.01 <br />L18137- 1405211549 Page 3 of 11 <br />@P, . = ir i4a^! <br />af i , <br />r r l <br />6 —'? --- -- u -- - <br />(-t– <br />-- Oa- <br />tr L — <br />-- L €k� <br />Iron, total recoverable <br />- - - -- -- <br />M200.7 ICP <br />1 <br />– <br />0.17 <br />mg /L <br />0.02 <br />0.05 <br />05113/14 18:45 <br />jjc <br />Selenium, potentially <br />M200.8 ICP -MS <br />2 <br />0.0076 <br />mg /L • <br />0.0002 <br />-0.0005 <br />05/09/14 22:58 <br />pmc <br />dissolved <br />Selenium, total <br />M200.8 ICP -MS <br />2 <br />0.0088 <br />mg /L <br />0.0002 <br />0.0005 <br />05/16/14 23:49 <br />pmc <br />recoverable <br />Wet Chemistry <br />I2C16 <br />i - f <br />Cic� <br />(,YAr�i <br />Residue, Filterable <br />SM2540C <br />1 <br />3620 <br />mg /L <br />10 <br />20 <br />05/12/14 16:13 <br />dcw <br />(TDS) @180C <br />REPIN.02.06.05.01 <br />L18137- 1405211549 Page 3 of 11 <br />