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www.energylab.cam <br />AedrticslFix kwoSaw 1JV <br />Client: Cotter Corporation <br />Project: Schwartz -GW 1/30/14 S27319 <br />Analyte Count <br />Method: E200.8 <br />Helena, MT 871 472 -0711 - Billings, MT 600 - 735 -4489 - Casper, WY 888- 235 -0515 <br />Gillette, WY 866-686 -1115 - Rapid City, SD 886 -672 -1225 - College Station, TX 888- 690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch Revised Date: 03/05/14 <br />Report Date: 02/18/14 <br />Work Order: C14020002 <br />Result Units <br />RL ° /.REC Low Limit High Limit RPD RPDLimit Qual <br />Analytical Run: ICPMS4- C_140205A <br />Sample ID: <br />Antimony <br />Arsenic <br />Copper <br />Lead <br />Silver <br />Thallium <br />ICV <br />6 Initial Calibration Verification Standard <br />0.0539 mg /L 0.0010 <br />0.0498 mg /L 0.0010 <br />0.0522 mg /L 0.0010 <br />0.0502 mg /L 0.0010 <br />0.0179 mg /L 0.0010 <br />0.0495 mg /L 0.0010 <br />108 <br />100 <br />104 <br />100 <br />90 <br />99 <br />90 <br />90 <br />90 <br />90 <br />90 <br />90 <br />110 <br />110 <br />110 <br />110 <br />110 <br />110 <br />02/05/14 18:37 <br />Method: <br />E200.8 <br />Batch: 40513 <br />Sample ID: <br />MB -40513 <br />6 Method Blank <br />Run: ICPMS4- C_140205A <br />02/05/14 21:19 <br />Antimony <br />ND mg /L <br />0.0002 <br />Arsenic <br />0.0006 mg /L <br />0.0002 <br />Copper <br />ND mg /L <br />6E -05 <br />Lead <br />ND mg /L <br />4E -05 <br />Silver <br />ND mg /L <br />0.0002 <br />Thallium <br />ND mg /L <br />6E -05 <br />Sample ID: <br />LCS3 -40513 <br />6 Laboratory Control Sample <br />Run: ICPMS4- C_140205A <br />02/05/14 21:23 <br />Antimony <br />0.57 mg /L <br />0.0010 <br />113 <br />85 <br />115 <br />Arsenic <br />0.49 mg /L <br />0.0010 <br />97 <br />85 <br />115 <br />Copper <br />0.44 mg /L <br />0.010 <br />88 <br />85 <br />115 <br />Lead <br />0.49 mg /L <br />0.0010 <br />98 <br />85 <br />115 <br />Silver <br />0.049 mg /L <br />0.010 <br />97 <br />85 <br />115 <br />Thallium <br />0.46 mg /L <br />0.00040 <br />93 <br />85 <br />115 <br />Sample ID: <br />014010890- 002AMS3 <br />6 Sample Matrix Spike <br />Run: ICPMS4- C_140205A <br />02/05/14 21:56 <br />Antimony <br />0.556 mg /L <br />0.0010 <br />111 <br />70 <br />130 <br />Arsenic <br />0.483 mg /L <br />0.0010 <br />97 <br />70 <br />130 <br />Copper <br />1.32 mg /L <br />0.0050 <br />85 <br />70 <br />130 <br />Lead <br />0.493 mg /L <br />0.0010 <br />98 <br />70 <br />130 <br />Silver <br />0.0464 mg /L <br />0.0010 <br />93 <br />70 <br />130 <br />Thallium <br />0.458 mg /L <br />0.00050 <br />92 <br />70 <br />130 <br />Sample ID: <br />C14010890- 002AMSD3 <br />6 Sample Matrix Spike Duplicate <br />Run: ICPMS4- C_140205A <br />02/05/14 21:59 <br />Antimony <br />0.557 mg /L <br />0.0010 <br />111 <br />70 <br />130 <br />0.2 <br />20 <br />Arsenic <br />0.484 mg /L <br />0.0010 <br />97 <br />70 <br />130 <br />0.4 <br />20 <br />Copper <br />1.31 mg /L <br />0.0050 <br />84 <br />70 <br />130 <br />0.5 <br />20 <br />Lead <br />0.499 mg /L <br />0.0010 <br />99 <br />70 <br />130 <br />1.1 <br />20 <br />Silver <br />0.0497 mg /L <br />0.0010 <br />99 <br />70 <br />130 <br />6.9 <br />20 <br />Thallium <br />0.468 mg /L <br />0.00050 <br />94 <br />70 <br />130 <br />2.2 <br />20 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 11 of 20 <br />