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AOZ Laboratories, Inc. <br />Golder Associates ACZ Sample ID: L113O7 -02 <br />Project ID: 10381640A Date Sampled: 03126113 00.00 <br />Sample ID: MW -7 265.0 -266.7 FT Date Received: 03127113 <br />Sample Matrix: Soil <br />Soil Analysis <br />Alkalinity (1312 DI) <br />SM2320B - Titration <br />Conductivity @25C <br />SM2510B <br />3.510 <br />mmhos /cm <br />0.001 <br />0.01 <br />04/08/13 17:01 <br />me <br />pH, (1312) <br />M9045D/M9040C <br />CaCO3 <br />pH <br />10.1 <br />units <br />0.1 <br />0.1 <br />04/03/13 0:00 <br />cdb <br />pH measured at <br />20 <br />22.1 <br />C <br />0.1 <br />0.1 <br />04/03/13 0:00 <br />cdb <br />pH, (1312-DI) <br />M9045D/M9040C <br />20 <br />04/04/13 0:00 <br />abm <br />Total Alkalinity <br />66 <br />pH <br />mg /L <br />9.8 <br />units <br />0.1 <br />0.1 <br />04/03/13 0:00 <br />cdb <br />pH measured at <br />22.1 <br />C <br />0.1 <br />0.1 <br />04/03/13 0:00 <br />cdb <br />pH, Saturated Paste <br />EPA 600/2 -78 -054, section 3.2.2 <br />10.7 <br />units <br />0.1 <br />0.1 <br />04/08/13 17:01 <br />me <br />Solids, Percent <br />CLPSOW390, PART F, D -98 <br />99.5 <br />% <br />0.1 <br />0.5 <br />04/01/13 21:00 <br />mjj <br />Soil Preparation <br />Fluoride (1312 DI) <br />SM4500F -C <br />0.1 <br />B <br />mg /L <br />0.1 <br />0.5 <br />'Parameter <br />EPA Method <br />Result Qual <br />XQ Units <br />MDL <br />POL <br />Date <br />Analyst <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />calc <br />Nitrate /Nitrite as N <br />M353.2 - Automated Cadmium <br />0.05 <br />04/01/13 17:07 <br />mjj <br />C <br />0.1 <br />04/03/13 22:54 <br />pjb <br />(1312 -DI) <br />Reduction <br />Crush and Pulverize <br />EPA - 600/2 -78 -054 3.1.3 <br />Nitrite as N (1312 -DI) <br />04/05/13 12:11 <br />mjj <br />(Ring & Puck) <br />mg /L <br />0.01 <br />0.05 <br />04/03/13 22:54 <br />pjb <br />Reduction <br />Digestion - Hot Plate <br />M3050B ICP -MS <br />04/08/13 21:33 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />mg /L <br />10 <br />20 <br />04/08/13 21:33 <br />me <br />Saturated Paste <br />USDA No. 60 (2) <br />04/08/13 12:53 <br />me <br />Extraction <br />Sulfate (1312 DI) <br />D516 -02 - Turbidimetric <br />25 <br />mg /L <br />1 <br />5 <br />Synthetic Precip. <br />M1312 <br />04/04/13 0:00 <br />mjj /cdb <br />Leaching Procedure <br />Synthetic Precip. <br />M1312, DI Water <br />04/03/13 0:37 <br />mjj /cdb <br />Leaching Procedure <br />Wet Chemistry <br />Alkalinity (1312 DI) <br />SM2320B - Titration <br />Bicarbonate as <br />5 <br />B <br />mg /L <br />2 <br />20 <br />04/04/13 0:00 <br />abm <br />CaCO3 <br />Carbonate as CaCO3 <br />61 <br />mg /L <br />2 <br />20 <br />04/04/13 0:00 <br />abm <br />Hydroxide as CaCO3 <br />U <br />* mg /L <br />2 <br />20 <br />04/04/13 0:00 <br />abm <br />Total Alkalinity <br />66 <br />mg /L <br />2 <br />20 <br />04/04/13 0:00 <br />abm <br />Chloride (1312 DI) <br />SM4500CI -E <br />20 <br />* mg /L <br />1 <br />5 <br />04/08/13 14:58 <br />mpb <br />Conductivity @25C <br />SM2510B <br />212 <br />* umhos /cm <br />1 <br />10 <br />04/04/13 15:32 <br />abm <br />(1312 -DI) <br />Fluoride (1312 DI) <br />SM4500F -C <br />0.1 <br />B <br />mg /L <br />0.1 <br />0.5 <br />04/04/13 15:02 <br />abm <br />Nitrate (1312 DI) <br />Calculation: NO3NO2 minus NO2 <br />0.05 <br />B <br />mg /L <br />0.02 <br />0.1 <br />04/16/13 10:52 <br />calc <br />Nitrate /Nitrite as N <br />M353.2 - Automated Cadmium <br />0.05 <br />B <br />mg /L <br />0.02 <br />0.1 <br />04/03/13 22:54 <br />pjb <br />(1312 -DI) <br />Reduction <br />Nitrite as N (1312 -DI) <br />M353.2 - Automated Cadmium <br />U <br />mg /L <br />0.01 <br />0.05 <br />04/03/13 22:54 <br />pjb <br />Reduction <br />Residue, Filterable <br />SM2540C <br />120 <br />mg /L <br />10 <br />20 <br />04/04/13 17:32 <br />khw <br />(TDS) @180C (1312) <br />Sulfate (1312 DI) <br />D516 -02 - Turbidimetric <br />25 <br />mg /L <br />1 <br />5 <br />04/09/13 16:12 <br />bsu <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 5 of 54 <br />