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AC3Z Laboratories, Inc. <br />'377o e...;- r^n nne07 innm ooA 9,401 <br />Golder Associates ACZ Sample ID: L11307 -01 <br />Project ID: 10381640A Date Sampled: 03126113 00:00 <br />Sample ID: CKD -1 15.0 -19.5 FT Date Received: 03127113 <br />Sample Matrix: Soil <br />Soil Analysis <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 3 of 54 <br />Conductivity @25C <br />SM2510B <br />25.600 <br />* mmhos /cm <br />0.001 <br />0.01 <br />04/08/13 15:34 <br />me <br />pH, (1312) <br />M9045D/M9040C <br />pH <br />12.5 <br />units <br />0.1 <br />0.1 <br />04/03/13 0:00 <br />cdb <br />pH measured at <br />22.1 <br />C <br />0.1 <br />0.1 <br />04/03/13 0:00 <br />cdb <br />pH, (1312 -DI) <br />M9045D/M9040C <br />pH <br />12.5 <br />units <br />0.1 <br />0.1 <br />04/02/13 0:00 <br />cdb <br />pH measured at <br />22.1 <br />C <br />0.1 <br />0.1 <br />04/02/13 0:00 <br />cdb <br />pH, Saturated Paste <br />EPA 600/2 -78 -054, section 3.2.2 <br />12.8 <br />units <br />0.1 <br />0.1 <br />04/08/13 15:34 <br />me <br />Solids, Percent <br />CLPSOW390, PART F, D -98 <br />99.6 <br />* % <br />0.1 <br />0.5 <br />04/01/13 19:15 <br />mjj <br />Soil Preparation <br />Parameter---- <br />EPA Method <br />Date <br />Analyst <br />Air Dry at 34 Degrees <br />USDA No. 1, 1972 <br />04/01/13 17:00 <br />mjj <br />C <br />Crush and Pulverize <br />EPA - 600/2 -78 -054 3.1.3 <br />04/05/13 12:00 <br />mjj <br />(Ring & Puck) <br />Digestion - Hot Plate <br />M3050B ICP -MS <br />04/08/13 17:13 <br />me <br />Digestion - Hot Plate <br />M3050B ICP <br />04/08/13 17:13 <br />me <br />Saturated Paste <br />USDA No. 60 (2) <br />04/08/13 10:00 <br />me <br />Extraction <br />Synthetic Precip. <br />M1312 <br />04/03/13 22:00 <br />mjj /cdb <br />Leaching Procedure <br />Synthetic Precip. <br />M1312, DI Water <br />04/02/13 21:52 <br />mjj /cdb <br />Leaching Procedure <br />Wet Chemistry <br />Parameter <br />EPA Method <br />Result <br />Qual XO Units <br />MDL <br />• w <br />Date <br />Analyst <br />Alkalinity (1312 DI) <br />SM2320B - Titration <br />Bicarbonate as <br />U mg /L <br />2 <br />20 <br />04/09/13 0:00 <br />Ijr <br />CaCO3 <br />Carbonate as CaCO3 <br />122 <br />mg /L <br />2 <br />20 <br />04/09/13 0:00 <br />Ijr <br />Hydroxide as CaCO3 <br />3290 <br />mg /L <br />2 <br />20 <br />04/09/13 0:00 <br />Ijr <br />Total Alkalinity <br />3420 <br />mg /L <br />2 <br />20 <br />04/09/13 0:00 <br />Ijr <br />Chloride (1312 DI) <br />SM4500CI -E <br />19 <br />B mg /L <br />5 <br />30 <br />04/08/13 14:58 <br />mpb <br />Conductivity @25C <br />SM2510B <br />12600 <br />umhos /cm <br />1 <br />10 <br />04/04/13 14:52 <br />abm <br />(1312 -DI ) <br />Fluoride (1312 DI) <br />SM450OF -C <br />2.4 <br />mg /L <br />0.1 <br />0.5 <br />04/04/13 14:51 <br />abm <br />Nitrate (1312 DI) <br />Calculation: NO3NO2 minus NO2 <br />0.30 <br />mg /L <br />0.02 <br />0.1 <br />04/16/13 10:52 <br />talc <br />Nitrate /Nitrite as N <br />M353.2 - Automated Cadmium <br />0.37 <br />mg /L <br />0.02 <br />0.1 <br />04/03/13 22:52 <br />pjb <br />(1312 -DI) <br />Reduction <br />Nitrite as N (1312 -DI) <br />M353.2 - Automated Cadmium <br />0.07 <br />mg /L <br />0.01 <br />0.05 <br />04/03/13 22:52 <br />pjb <br />Reduction <br />Residue, Filterable <br />SM2540C <br />4830 <br />mg /L <br />10 <br />20 <br />04/04/13 17:27 <br />khw <br />(TDS) @180C (1312) <br />Sulfate (1312 DI) <br />D516 -02 - Turbidimetric <br />1700 <br />mg /L <br />100 <br />500 <br />04/09/13 16:26 <br />bsu <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 3 of 54 <br />