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Analytical dzufelt(a),greenanalytical.com p: 970.247.4220 f: 970247.4227 75 Suttle Street Durango, CO 81303 <br />Laboratories <br />www.Green Analytical. com <br />GCC Energy, LLC Project: Quarterly <br />6473 CR 120 Project Name / Number: King I and II Reported: <br />Hesperus CO, 81326 Project Manager: Tom Bird 04/15/14 15:52 <br />General Chemistry - Quality Control <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch B403265 - General Prep - Wet Chem <br />Duplicate (B403265 -DUPl) <br />Source: 1403237 -01 <br />Prepared & Analyzed: 03/28/14 <br />pH <br />Reference (B403265 -SRMI) <br />7.79 <br />pH Units <br />7.74 <br />Prepared & Analyzed: 03/28/14 <br />0.644 20 <br />pH <br />Batch B404080 - General Prep - Wet Chem <br />8.78 <br />pH Units <br />9.10 96.5 <br />90 -110 <br />Blank (B404080 -BLKI) <br />Prepared & Analyzed: 04/08/14 <br />Alkalinity, Total <br />LCS (B404080 -BSI) <br />ND <br />10.0 <br />mg/L <br />Prepared & Analyzed: 04/08/14 <br />Alkalinity, Total <br />LCS Dup (B404080 -BSDI) <br />101 <br />10.0 <br />mg/L <br />100 101 <br />Prepared & Analyzed: 04/08/14 <br />85 -115 <br />Alkalinity, Total <br />Batch B404109 - General Prep - Wet Chem <br />103 <br />10.0 <br />mg/L <br />100 103 <br />85 -115 1.96 20 <br />Blank (B404109 -BLKI) <br />Prepared & Analyzed: 04/10/14 <br />Sulfate <br />LCS (B404109 -BSI) <br />ND <br />10.0 <br />mg/L <br />Prepared & Analyzed: 04/10/14 <br />Sulfate <br />LCS Dup (B404lO9 -BSDI) <br />53.0 <br />10.0 <br />mg/L <br />50.0 106 <br />Prepared & Analyzed: 04/10/14 <br />85 -115 <br />Sulfate <br />53.0 <br />10.0 <br />mg/L, <br />50.0 106 <br />85 -115 0.00 20 <br />Green Analytical Laboratories <br />Debbie Zufelt, Reports Manager <br />The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. In no event <br />shall Green Analytical Laboratories be liable for incidental or consequential damages. <br />GALS liability, and clients exclusive remedy for any claim arising, shall be limited to the <br />amount paid by client for analyses. All claims, including those for negligence and any other <br />cause whatsoever, shall be deemed waived unless made in writing and received within <br />thirty days after completion of the applicable service. <br />Page 7 of 12 <br />