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FM www.energylab.cor1 Helena, MT 877- 472 -0711 • Billings, MT 800 -735 -4489 • Casper, WY 888- 235 -0515 <br />Ewoh=2=1JV Gillette, WY 866- 686 -7175 • Rapid City, SD 886 -672 -1225 • College Station, TX 888- 690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 02/03/14 <br />Project: Schwartz GW 12/23/13 S27306 Work Order: C13120854 <br />Analyte Count Result Units RL ° /.REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.7 <br />476 <br />mg /L <br />0.000520 <br />mg /L <br />464 <br />Analytical Run: ICP4- C_131227A <br />Sample ID: ICV <br />10 Initial Calibration Verification Standard <br />500 <br />mg /L <br />12/27/13 12:43 <br />Aluminum <br />4.95 <br />mg /L <br />0.10 <br />99 <br />95 <br />105 <br />Barium <br />1.00 <br />mg /L <br />0.10 <br />100 <br />95 <br />105 <br />Calcium <br />50.3 <br />mg /L <br />0.50 <br />101 <br />95 <br />105 <br />Iron <br />5.00 <br />mg /L <br />0.030 <br />100 <br />95 <br />105 <br />Magnesium <br />50.2 <br />mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Manganese <br />4.89 <br />mg /L <br />0.010 <br />98 <br />95 <br />105 <br />Molybdenum <br />0.988 <br />mg /L <br />0.10 <br />99 <br />95 <br />105 <br />Potassium <br />49.6 <br />mg /L <br />0.50 <br />99 <br />95 <br />105 <br />Sodium <br />50.1 <br />mg /L <br />0.50 <br />100 <br />95 <br />105 <br />Zinc <br />0.954 <br />mg /L <br />0.010 <br />95 <br />95 <br />105 <br />Sample ID: ICSA <br />Aluminum <br />Barium <br />Calcium <br />Iron <br />Magnesium <br />Manganese <br />Molybdenum <br />Potassium <br />Sodium <br />Zinc <br />Sample ID: ICSAB <br />Aluminum <br />Barium <br />Calcium <br />I ron <br />Magnesium <br />Manganese <br />Molybdenum <br />Potassium <br />Sodium <br />Zinc <br />10 Interference Check Sample A <br />476 <br />mg /L <br />0.000520 <br />mg /L <br />464 <br />mg /L <br />176 <br />mg /L <br />500 <br />mg /L <br />- 0.00689 <br />mg /L <br />0.00385 <br />mg /L <br />0.00360 <br />mg /L <br />-0.294 <br />mg /L <br />0.000420 <br />mg /L <br />10 Interference Check Sample AB <br />476 <br />mg /L <br />0.465 <br />mg /L <br />465 <br />mg /L <br />177 <br />mg /L <br />501 <br />mg /L <br />0.442 <br />mg /L <br />0.00146 <br />mg /L <br />- 0.00757 <br />mg /L <br />-0.399 <br />mg /L <br />0.839 <br />mg /L <br />0.10 <br />0.10 <br />0.50 <br />0.030 <br />0.50 <br />0.010 <br />0.10 <br />0.50 <br />0.50 <br />0.010 <br />0.10 <br />0.10 <br />0.50 <br />0.030 <br />0.50 <br />0.010 <br />0.10 <br />0.50 <br />0.50 <br />0.010 <br />Method: E200.7 <br />80 <br />120 <br />93 <br />Sample ID: MB- 131227A <br />10 Method Blank <br />88 <br />80 <br />Aluminum <br />ND <br />mg /L <br />0.009 <br />Barium <br />ND <br />mg /L <br />0.0002 <br />Calcium <br />ND <br />mg /L <br />0.02 <br />Iron <br />0.002 <br />mg /L <br />0.002 <br />Magnesium <br />0.04 <br />mg /L <br />0.01 <br />Manganese <br />ND <br />mg /L <br />0.0010 <br />Molybdenum <br />ND <br />mg /L <br />0.003 <br />Potassium <br />ND <br />mg /L <br />0.04 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />95 <br />80 <br />120 <br />93 <br />80 <br />120 <br />88 <br />80 <br />120 <br />100 <br />80 <br />120 <br />95 <br />80 <br />120 <br />93 <br />80 <br />120 <br />93 <br />80 <br />120 <br />89 <br />80 <br />120 <br />100 <br />80 <br />120 <br />88 <br />80 <br />120 <br />84 80 120 <br />Run: ICP4- C_131227A <br />ND - Not detected at the reporting limit. <br />12/27/13 12:57 <br />12/27/13 13:01 <br />Batch: R182102 <br />12/27/13 13:19 <br />Page 12 of 31 <br />