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ADZ Laboratories, Inc. <br />2773 Downhill Dnve Steamhnat Snnnos Cn R04R7 /R= 3.44-.549.4 <br />Star Mine Operations LLC <br />Project ID: <br />Sample ID: UG -3 <br />Wet Chemistry <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />L16818-03 <br />02112114 06:40 <br />02113/14 <br />Surface Water <br />earameteiav_i„ena. <br />s <br />iluti 7i <br />ftesult <br />p . <br />i:(• =rfiiis li <br />4. UL <br />IrlL <br />Date <br />Fluoride <br />Alkalinity as CaCC3 <br />SM2320B - Titration <br />0.3 B <br />mg /L <br />0.1 <br />0.5 <br />02/24/14 16 31 <br />abd <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />Bicarbonate as <br />203 <br />1 <br />60 <br />7 <br />mg /L <br />2 <br />20 <br />02/17/14 0.00 <br />abd <br />CaCC3 <br />02/20/14 13:48 <br />id <br />filter) <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Hydroxide as CaCO3 <br />1 <br />mfm <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Total Alkalinity <br />1 <br />60 <br />M353 2 - H2SO4 preserved <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Cation -Anion Balance <br />Calculation <br />pH (lab) <br />SM4500H+ B <br />Cation -Anion Balance <br />pH <br />2.7 <br />7.9 H <br />% <br />0.1 <br />0.1 <br />02/28/14 9.32 <br />talc <br />Sum of Anions <br />1 <br />5.4 <br />C <br />meq /L <br />0.1 <br />0.5 <br />02/28/14 9:32 <br />talc <br />Sum of Cations <br />1 <br />U * <br />5.7 <br />0.01 <br />meq /L <br />0.1 <br />0.5 <br />02/28/14 9.32 <br />talc <br />Chloride <br />SM4500CI -E <br />1 <br />U <br />mg /L <br />1 <br />5 <br />02/20/14 19 04 <br />mpb <br />Conductivity @25C <br />SM2510B <br />1 <br />534 <br />02/25/14 11:09 <br />umhos /cm <br />1 <br />10 <br />02/17/14 20:56 <br />abd <br />Cyanide, total <br />M335 4 - Colorimetnc w/ distillation <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />02/19/14 23:34 <br />pjb <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetric <br />0.5 <br />abd <br />U <br />mg /L <br />0.003 <br />0.01 <br />02/19/14 23:15 <br />pjb <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />L16818- 1402281029 Page 7 of 29 <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.3 B <br />mg /L <br />0.1 <br />0.5 <br />02/24/14 16 31 <br />abd <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />203 <br />mg /L <br />1 <br />7 <br />02/28/14 9.32 <br />talc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />02/20/14 13:48 <br />id <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />02/14/14 11.42 <br />mfm <br />& Acidification <br />Nitrate /Nitrite as N <br />M353 2 - H2SO4 preserved <br />1 <br />0.11 <br />mg /L <br />0.02 <br />0.1 <br />02/22/14 0.39 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />7.9 H <br />units <br />0.1 <br />0.1 <br />02/17/14 0:00 <br />abd <br />pH measured at <br />1 <br />22 <br />C <br />0.1 <br />0.1 <br />02/17/14 0.00 <br />abd <br />Phosphorus, ortho <br />M365 1 - Automated Ascorbic Acid <br />1 <br />U * <br />mg /L <br />0.01 <br />0.05 <br />02/13/14 21.34 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />360 H <br />mg /L <br />10 <br />20 <br />02/25/14 11:09 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />U * <br />mg /L <br />5 <br />20 <br />02/19/14 11:48 <br />abd <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516- 02- Turbidimetric <br />10 <br />199 <br />mg /L <br />10 <br />50 <br />02/21/1413:48 <br />bsu <br />TDS (calculated) <br />Calculation <br />350 <br />mg /L <br />10 <br />50 <br />02/28/14 9.32 <br />talc <br />TDS (ratio - <br />calculation <br />1.03 <br />02/28/14 9 32 <br />talc <br />measured /calculated) <br />For Cadmium by ICPMS, <br />the value in the MDL <br />field is the client's requested <br />reporting limit. <br />A "U" qualifier denotes cadmium was not detected above this level. <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />L16818- 1402281029 Page 7 of 29 <br />