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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat S'DnnoS. CO 80487 (800) 334 -5493 <br />Star Mine Operations LLC ACZ Sample ID: <br />L16818 -01 <br />Project ID: Date Sampled: <br />02112114 06:15 <br />Sample ID: UG -1 Date Received: <br />02113114 <br />Sample Matrix: <br />Surface Water <br />Wet Chemistry <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />L16818- 1402281029 Page 3 of 29 <br />ziliution <br />KOSUlt <br />Qual <br />AQ 1 <br />.;.DL <br />R <br />Date <br />Analyst <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />0.2 B <br />mg /L <br />0.1 <br />0.5 <br />02/24/141619 <br />abd <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />Bicarbonate as <br />175 <br />1 <br />60 <br />7 <br />mg /L <br />2 <br />20 <br />02/17/14 0.00 <br />abd <br />CaCO3 <br />02/20/14 13:36 <br />id <br />filter) <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Hydroxide as CaCO3 <br />1 <br />mfm <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0.00 <br />abd <br />Total Alkalinity <br />1 <br />60 <br />M353.2 - H2SO4 preserved <br />mg /L <br />2 <br />20 <br />02/17/14 0.00 <br />abd <br />Cation -Anion Balance <br />Calculation <br />pH (lab) <br />SM4500H+ B <br />Cation -Anion Balance <br />pH <br />-1.3 <br />8.2 H <br />% <br />0.1 <br />0.1 <br />02/28/14 9:32 <br />calc <br />Sum of Anions <br />1 <br />3.9 <br />C <br />meq /L <br />0.1 <br />0.5 <br />02/28/14 9:32 <br />calc <br />Sum of Cations <br />1 <br />U <br />3.8 <br />0.01 <br />meq /L <br />0.1 <br />0.5 <br />02/28/14 9.32 <br />calc <br />Chloride <br />SM45000I -E <br />1 <br />U <br />mg /L <br />1 <br />5 <br />02/20/1418.59 <br />mpb <br />Conductivity @25C <br />SM2510B <br />1 <br />400 <br />02/25/14 11.06 <br />umhos /cm <br />1 <br />10 <br />02/17/14 20:33 <br />abd <br />Cyanide, total <br />M335 4 - Colorimetnc w/ distillation <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />02/18/14 13:29 <br />mss2 <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetric <br />0.5 <br />abd <br />U <br />mg /L <br />0.003 <br />0.01 <br />02/19/14 23'12 <br />p1b <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />L16818- 1402281029 Page 3 of 29 <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.2 B <br />mg /L <br />0.1 <br />0.5 <br />02/24/141619 <br />abd <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />175 <br />mg /L <br />1 <br />7 <br />02/28/14 9,32 <br />calc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />02/20/14 13:36 <br />id <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />02/14/14 11.42 <br />mfm <br />& Acidification <br />Nitrate /Nitrite as N <br />M353.2 - H2SO4 preserved <br />1 <br />1.04 <br />mg /L <br />0.02 <br />0.1 <br />02/22/14 0:35 <br />plb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.2 H <br />units <br />0.1 <br />0.1 <br />02/17/14 0:00 <br />abd <br />pH measured at <br />1 <br />21 <br />C <br />0.1 <br />0.1 <br />02/17/14 0.00 <br />abd <br />Phosphorus, ortho <br />M3651- Automated Ascorbic Acid <br />1 <br />U <br />mg /L <br />0.01 <br />0.05 <br />02/13/1421'29 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />260 H <br />mg /L <br />10 <br />20 <br />02/25/14 11.06 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />U <br />mg /L <br />5 <br />20 <br />02/19/14 11:46 <br />abd <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516- 02- Turbidimetric <br />5 <br />129 <br />mg /L <br />5 <br />25 <br />02/21/1413.46 <br />bsu <br />TDS (calculated) <br />Calculation <br />249 <br />mg /L <br />10 <br />50 <br />02/28/14 9:32 <br />calc <br />TDS (ratio - <br />Calculation <br />1.04 <br />02/28/14 9'32 <br />calc <br />measured /calculated) <br />For Cadmium by ICPMS, the value in the MDL <br />field is the client's requested <br />reporting limit. <br />A "U" qualifier denotes <br />cadmium was not detected above this level. <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />L16818- 1402281029 Page 3 of 29 <br />