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ACZ Laboratories, Inc. <br />0770 n..,. -i-11 n.,, 04i......4.. 4 c....... nn 0-07 /0nn1 00.f cnn0 <br />Star Mine Operations LLC <br />Project ID: <br />Sample ID: SW -2 <br />ACZ Sample ID <br />Date Sampled <br />Date Received <br />Sample Matrix <br />L16817-01 <br />02112114 09:30 <br />02113/14 <br />Surface Water <br />Sodium, total <br />M200.7ICP <br />1 <br />2.8 <br />mg /L <br />0.2 <br />1 <br />02/19/14 17.05 <br />aeb <br />Thallium, dissolved <br />M200 s ICP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />02/21/14 1.28 <br />msh <br />Thallium, total <br />M200 8 ICP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />02/25/14 2.18 <br />pmc <br />Uranium, dissolved <br />M200.8 ICP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />02/21/14 1:28 <br />msh <br />Uranium, total <br />M200.8 ICP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />02/25/14 2.18 <br />pmc <br />Vanadium, dissolved <br />M200.71CP <br />1 <br />U <br />mg /L <br />0.005 <br />0.03 <br />02/18/14 16.25 <br />aeb <br />Vanadium, total <br />M200.71CP <br />1 <br />U <br />mg /L <br />0.005 <br />0.03 <br />02/19/14 17.05 <br />aeb <br />Zinc, dissolved <br />M200 7 lCP <br />1 <br />0.11 <br />mg /L <br />0.01 <br />0.05 <br />02/18/14 16:25 <br />aeb <br />Zinc, total <br />M200 7 ICP <br />1 <br />0.13 <br />mg /L <br />0.01 <br />0.05 <br />02/19/14 17:05 <br />aeb <br />Wet Chemistry <br />Parameter <br />EPA Method Dilution <br />Result <br />Qual <br />XQ Units <br />MDL <br />PQL <br />Date Analyst' <br />Alkalinity as CaCO3 <br />SM2320B- Titration <br />Bicarbonate as <br />1 <br />40 <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0:00 <br />abd <br />Hydroxide as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />02/17/14 0.00 <br />abd <br />Total Alkalinity <br />1 <br />40 <br />mg /L <br />2 <br />20 <br />02/17/14 0.00 <br />abd <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />-5.0 <br />% <br />02/28/14 9:20 <br />talc <br />Sum of Anions <br />2.1 <br />meq /L <br />0.1 <br />0.5 <br />02/28/14 9:20 <br />talc <br />Sum of Cations <br />1.9 <br />meq /L <br />0.1 <br />0.5 <br />02/28/14 9.20 <br />talc <br />Chloride <br />SM450oci -E <br />1 <br />U <br />mg /L <br />1 <br />5 <br />02/20/14 18 59 <br />mpb <br />Conductivity @25C <br />SM2510B <br />1 <br />227 <br />umhos /cm <br />1 <br />10 <br />02/17/14 19:46 <br />abd <br />Cyanide, total <br />M335 4 - Colonmetnc w/ distillation <br />0.5 <br />U <br />* mg /L <br />0.003 <br />0.01 <br />02/18/14 13:22 <br />mss2 <br />Cyanide, WAD <br />SM4500 -CN I- Colonmetric <br />0.5 <br />U <br />* mg /L <br />0.003 <br />0.01 <br />02/19/14 23.05 <br />pjb <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.2 <br />B <br />mg /L <br />0.1 <br />0.5 <br />02/24/1415:45 <br />abd <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />90 <br />mg /L <br />1 <br />7 <br />02/28/14 9:20 <br />talc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />02/20114 1259 <br />id <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />02/14/14 11.39 <br />mfm <br />& Acidification <br />Nitrate /Nitrite as N <br />M353.2 - H2SO4 preserved <br />1 <br />0.15 <br />mg /L <br />0.02 <br />0.1 <br />02/22/14 0:25 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8 <br />H <br />units <br />0.1 <br />0.1 <br />02/17/14 0.00 <br />abd <br />pH measured at <br />1 <br />21 <br />C <br />0.1 <br />0.1 <br />02/17/14 0 00 <br />abd <br />Phosphorus, ortho <br />M365 1 - Automated Ascorbic Acid <br />1 <br />U <br />mg /L <br />0.01 <br />0.05 <br />02/13/14 21:20 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />140 <br />mg /L <br />10 <br />20 <br />02/18/14 16.20 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />U <br />mg /L <br />5 <br />20 <br />02/19/14 11.41 <br />abd <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516- 02- Turbidimetnc <br />5 <br />59.7 <br />mg /L <br />5 <br />25 <br />02/19/1416:52 <br />bsu <br />TDS (calculated) <br />Calculation <br />126 <br />mg /L <br />10 <br />50 <br />02/28/14 9.20 <br />talc <br />TDS (ratio - <br />Calculation <br />1.11 <br />02/28/14 9.20 <br />talc <br />measured /calculated) <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />L16817- 1402281027 Page 4 of 49 <br />