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ACZ Laboratories, Inc. <br />Star Mine Operations LLC ACZ Project ID: L16199 <br />Selenium, dissolved <br />ACZ ID Type <br />Analyzed <br />M200.8 ICP -MS <br />PCNISCN Qc <br />Sample <br />Found <br />Units <br />Rec <br />Lower <br />Upper RPD Limit qual <br />WG357502 <br />11131217 -11 <br />WG3574461CV <br />ICV <br />01/07/1422:42 <br />MS140106 -2 <br />.05 <br />ASD <br />.05035 <br />mg /L <br />100.7 <br />WG3575021CV <br />ICV <br />01/10/1421:09 <br />MS140106 -2 <br />.05 <br />01/06/1417:46 <br />.0505 <br />mg /L <br />101 <br />90 <br />110 <br />WG357502ICB <br />ICB <br />01/10/14 21:12 <br />LRB <br />01/07/1422:49 <br />130 <br />U <br />mg /L <br />U <br />- 0.0003 <br />0.0003 <br />WG357502LFB <br />LFB <br />01/10/14 21:53 <br />MS140103 -2 <br />.05005 <br />MS140103 -2 <br />.04997 <br />mg /L <br />99.8 <br />85 <br />115 <br />L16199 -01AS <br />AS <br />01/10/1422:16 <br />MS140103 -2 <br />.05005 <br />.0006 <br />.05673 <br />mg /L <br />112.1 <br />70 <br />130 <br />L16199 -01ASD <br />ASD <br />01/10/1422:19 <br />MS140103 -2 <br />.05005 <br />.0006 <br />.0576 <br />mg /L <br />113.9 <br />70 <br />130 1.52 20 <br />L16227 -02AS <br />AS <br />01/10/14 23:14 <br />MS140103 -2 <br />.1001 <br />.0064 <br />.10916 <br />mg /L <br />102.7 <br />70 <br />130 <br />L16227 -02ASD <br />ASD <br />01/10/1423:17 <br />MS140103 -2 <br />.1001 <br />.0064 <br />.11486 <br />mg /L <br />108.4 <br />70 <br />130 5.09 20 <br />Selenium, total M200.8 ICP -MS <br />W G357446 <br />01/06/1416:03 <br />11131230 -1 <br />42.8 <br />ICB <br />01/06/1416:09 <br />99.2 <br />U <br />LFB <br />01/06/1416:22 <br />11131217 -11 <br />WG3574461CV <br />ICV <br />01/07/1422:42 <br />MS140106 -2 <br />.05 <br />ASD <br />.05035 <br />mg /L <br />100.7 <br />90 <br />110 <br />WG3574461CB <br />ICB <br />01/07/1422:46 <br />01/06/1417:46 <br />11131217 -11 <br />1071.4 <br />U <br />mg /L <br />130 <br />- 0.0003 <br />0.0003 <br />WG357372LRB <br />LRB <br />01/07/1422:49 <br />130 <br />1189 <br />mg /L <br />U <br />mg /L <br />115 0.42 20 <br />- 0.00022 <br />0.00022 <br />WG357372LFB <br />LFB <br />01/07/1422:52 <br />MS140103 -2 <br />.05005 <br />8.7 30.54 <br />.04958 <br />mg /L <br />99.1 <br />85 <br />115 <br />L16199 -07LFM <br />LFM <br />01/07/1423:28 <br />MS140103 -2 <br />.05005 <br />.0004 <br />.05066 <br />mg /L <br />100.4 <br />70 <br />130 <br />L16199- 07LFMD <br />LFMD <br />01/07/1423:31 <br />MS140103 -2 <br />.05005 <br />.0004 <br />.05086 <br />mg /L <br />100.8 <br />70 <br />130 0.39 20 <br />L16200 -05LFM <br />LFM <br />01/08/14 0:09 <br />MS140103 -2 <br />.05005 <br />.0002 <br />.05267 <br />mg /L <br />104.8 <br />70 <br />130 <br />L16200- 05LFMD <br />LFMD <br />01/08/14 0:13 <br />MS140103 -2 <br />.05005 <br />.0002 <br />.05207 <br />mg /L <br />103.6 <br />70 <br />130 1.15 20 <br />Silica, dissolved <br />WG367326 <br />WG3573261CV <br />WG357326ICB <br />WG357326LFB <br />L16199 -01AS <br />L16199 -01ASD <br />L16227 -01AS <br />L16227 -01ASD <br />Silica, total <br />WG367306 <br />WG3573061CV <br />WG357306ICB <br />WG357236LRB <br />WG357236LFB <br />L16199 -01LFM <br />L16199 -01 LFMD <br />WG357522 <br />WG3575221CV <br />WG357522ICB <br />WG357484LRB <br />WG357484LFB <br />L1620G -01LFM <br />L1620G -01 LFMD <br />M200.7 ICP <br />ICV <br />01/06/1416:03 <br />11131230 -1 <br />42.8 <br />ICB <br />01/06/1416:09 <br />99.2 <br />U <br />LFB <br />01/06/1416:22 <br />11131217 -11 <br />21.428 <br />AS <br />01/06/1416:44 <br />11131217 -11 <br />21.428 <br />ASD <br />01/06/1416:47 <br />11131217 -11 <br />21.428 <br />AS <br />01/06/1417:43 <br />11131217 -11 <br />1071.4 <br />ASD <br />01/06/1417:46 <br />11131217 -11 <br />1071.4 <br />M200.7 ICP <br />ICV <br />44.14 <br />mg /L <br />103.1 <br />95 <br />105 <br />99.2 <br />U <br />mg /L <br />ICB <br />-1.2 <br />1.2 <br />22.02 <br />mg /L <br />102.8 <br />85 <br />115 <br />8.5 <br />30.62 <br />mg /L <br />103.2 <br />85 <br />115 <br />8.5 <br />30.47 <br />mg /L <br />102.5 <br />85 <br />115 0.49 20 <br />130 <br />1194 <br />mg /L <br />99.3 <br />85 <br />115 <br />130 <br />1189 <br />mg /L <br />98.8 <br />85 <br />115 0.42 20 <br />ICV <br />01/06/1418:12 <br />11131219 -1 <br />42.8 <br />42.44 <br />mg /L <br />99.2 <br />95 <br />105 <br />ICB <br />01/06/1418:18 <br />U <br />mg /L <br />-1.2 <br />1.2 <br />LRB <br />01/06/1418:31 <br />U <br />mg /L <br />-0.88 <br />0.88 <br />LFB <br />01/06/1418:34 <br />11131217 -11 <br />21.428 <br />20.61 <br />mg /L <br />96.2 <br />85 <br />115 <br />LFM <br />01/06/1419:09 <br />11131217 -11 <br />21.428 <br />8.7 30.13 <br />mg /L <br />100 <br />70 <br />130 <br />LFMD <br />01/06/1419:12 <br />11131217 -11 <br />21.428 <br />8.7 30.54 <br />mg /L <br />101.9 <br />70 <br />130 1.35 20 <br />ICV <br />01/09/1414:04 <br />11131219 -1 <br />42.8 <br />42.57 <br />mg /L <br />99.5 <br />95 <br />105 <br />ICB <br />01/09/1414:10 <br />U <br />mg /L <br />-1.2 <br />1.2 <br />LRB <br />01/09/1414:23 <br />U <br />mg /L <br />-0.88 <br />0.88 <br />LFB <br />01/09/1414:26 <br />11131217 -11 <br />21.428 <br />20.4 <br />mg /L <br />95.2 <br />85 <br />115 <br />LFM <br />01/09/1415:07 <br />11131217 -11 <br />21.428 <br />17.2 34.69 <br />mg /L <br />81.6 <br />70 <br />130 <br />LFMD <br />01/09/1415:10 <br />11131217 -11 <br />21.428 <br />17.2 34.82 <br />mg /L <br />82.2 <br />70 <br />130 0.37 20 <br />REPIN.01.06.05.01 Page 61 of 79 <br />