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ACZ Laboratories, Inc. <br />9774 1111 -hill rlr! „c Qf-1-f C-4- /-Yl RnA97 /4/1M 49e geno <br />Star Mine Operations LLC <br />Project ID: <br />Sample ID: UG -4 <br />ACZ Sample ID <br />Date Sampled <br />Date Received <br />Sample Matrix <br />L16199-04 <br />12/26/13 06.45 <br />12127/13 <br />Surface Water <br />Sodium, total <br />M200.71CP <br />1 <br />11.2 <br />mg /L <br />0.3 <br />2 <br />01/07/14 19:50 <br />aeb <br />Thallium, dissolved <br />M200.8 ICP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />01/10/14 22:35 <br />pmc <br />Thallium, total <br />M200.81CP -MS <br />1 <br />U <br />mg /L <br />0.0001 <br />0.0005 <br />01/07/14 23:08 <br />pmc <br />Uranium, dissolved <br />M200.81CP -MS <br />1 <br />0.0009 <br />mg /L <br />0.0001 <br />0.0005 <br />01/10/14 22:35 <br />pmc <br />Uranium, total <br />M200.81CP -MS <br />1 <br />0.0010 <br />mg /L <br />0.0001 <br />0.0005 <br />01/07/14 23:08 <br />pmc <br />Vanadium, dissolved <br />M200.71CP <br />1 <br />U <br />mg /L <br />0.005 <br />0.03 <br />01/06/14 17:02 <br />aeb <br />Vanadium, total <br />M200.71CP <br />1 <br />U <br />mg /L <br />0.005 <br />0.03 <br />01/07/14 19:50 <br />aeb <br />Zinc, dissolved <br />M200.71CP <br />1 <br />0.02 <br />B <br />mg /L <br />0.01 <br />0.05 <br />01/06/14 17:02 <br />aeb <br />Zinc, total <br />M200.71CP <br />1 <br />0.05 <br />mg /L <br />0.01 <br />0.05 <br />01/07/14 19:50 <br />aeb <br />Wet Chemistry <br />Parameter <br />EPA Method Dilution <br />Result <br />Qual <br />XQ Units <br />MDL <br />POL <br />Date Analyst <br />Alkalinity as CaCO3 <br />SM2320B- Titration <br />Bicarbonate as <br />1 <br />73 <br />mg /L <br />2 <br />20 <br />12/28/13 0:00 <br />dcw <br />CaCO3 <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />12/28/13 0:00 <br />dcw <br />Hydroxide as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />12/28/13 0:00 <br />dcw <br />Total Alkalinity <br />1 <br />73 <br />mg /L <br />2 <br />20 <br />12/28/13 0:00 <br />dcw <br />Cation -Anion Balance <br />Calculation <br />Cation -Anion Balance <br />-7.9 <br />% <br />01/15/14 11:50 <br />calc <br />Sum of Anions <br />4.1 <br />meq /L <br />0.1 <br />0.5 <br />01/15/14 11:50 <br />calc <br />Sum of Cations <br />3.5 <br />meq /L <br />0.1 <br />0.5 <br />01/15/14 11:50 <br />calc <br />Chloride <br />SM4500CI -E <br />1 <br />1 <br />B <br />* mg /L <br />1 <br />5 <br />01/09/1416:04 <br />tcd <br />Conductivity @25C <br />SM2510B <br />1 <br />405 <br />umhos /cm <br />1 <br />10 <br />12/28/13 2:45 <br />dcw <br />Cyanide, total <br />M335.4- Colorimetricw /distillation <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />01/06/14 16:05 <br />bsu <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetric <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />01/06/14 16:41 <br />bsu <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.3 <br />B <br />mg /L <br />0.1 <br />0.5 <br />01/04/1418:59 <br />khw <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />153 <br />mg /L <br />1 <br />7 <br />01/15/14 11:50 <br />calc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />01/03/14 14:01 <br />abd <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />01/02/14 14:00 <br />las <br />& Acidification <br />Nitrate /Nitrite as N <br />M353.2- H2SO4 preserved <br />1 <br />0.12 <br />* mg /L <br />0.02 <br />0.1 <br />01/07/14 23:40 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.2 <br />H <br />units <br />0.1 <br />0.1 <br />12/28/13 0:00 <br />dcw <br />pH measured at <br />1 <br />22 <br />C <br />0.1 <br />0.1 <br />12/28/13 0:00 <br />dcw <br />Phosphorus, ortho <br />M365.1- Automated Ascorbic Acid <br />1 <br />0.01 <br />B <br />mg /L <br />0.01 <br />0.05 <br />12/27/1323:06 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />250 <br />mg /L <br />10 <br />20 <br />12/30/13 14:14 <br />dcw <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />8 <br />B <br />mg /L <br />5 <br />20 <br />12/30/13 11:48 <br />id <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516- 02- Turbidimetric <br />5 <br />123 <br />* mg /L <br />5 <br />25 <br />01/08/1413:28 <br />mpb <br />TDS (calculated) <br />Calculation <br />245 <br />mg /L <br />10 <br />50 <br />01/15/14 11:50 <br />calc <br />TDS (ratio - <br />Calculation <br />1,02 <br />01/15/14 11:50 <br />calc <br />measured /calculated) <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 17 of 79 <br />