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www.energylab.com Helena, MT 877- 472 -0711 - Billings, MT 800 - 735 -4489 - Casper, WY 888- 235 -0515 <br />Gillette, WY 866 -686 -7175 - Rapid City, SO 886 -672 -1225 - College Station, TX 888 -690 -2218 <br />QA /QC Summary Report <br />Prepared by Casper, WY Branch <br />Client: Cotter Corporation Report Date: 12/10/13 <br />Project: Schwartz SW 11/6/13 S27253 S27255 S27256 Work Order: C13110305 <br />Analyte <br />Count Result Units <br />RL <br />%REC <br />Low Limit High Limit <br />RPD <br />RPDLimit Qual <br />Method: <br />E200.7 <br />Initial Calibration Verification Standard <br />11/25/13 13:45 <br />Batch: R181147 <br />Sample ID: <br />LFB- 131122A 7 Laboratory Fortified Blank <br />0.50 <br />104 <br />Run: ICP2- C_131122A <br />11/22/13 14:20 <br />Sample ID: <br />C13110821- 005BMS2 7 Sample Matrix Spike <br />Run: ICP2- C_131122A <br />11/25/13 14:32 <br />11/22/13 20:35 <br />Aluminum <br />9.90 mg /L <br />0.14 <br />97 <br />70 130 <br />Sample ID: <br />Calcium <br />618 mg /L <br />1.0 <br />100 <br />70 130 <br />11/25/13 14:36 <br />Sodium <br />Iron <br />11.2 mg /L <br />0.030 <br />99 <br />70 130 <br />Method: <br />Magnesium <br />510 mg /L <br />1.0 <br />96 <br />70 130 <br />Batch: R181220 <br />Sample ID: <br />Manganese <br />10.4 mg /L <br />0.0024 <br />96 <br />70 130 <br />11/25/13 15:00 <br />Sodium <br />Potassium <br />463 mg /L <br />1.0 <br />89 <br />70 130 <br />Sample ID: <br />Zinc <br />9.70 mg /L <br />0.025 <br />95 <br />70 130 <br />11/25/13 15:04 <br />Sodium <br />Sample ID: <br />C13110821- 005BMSD2 7 Sample Matrix Spike Duplicate <br />0.50 <br />100 <br />Run: ICP2- C_131122A <br />11/22/13 20:39 <br />Aluminum <br />9.90 mg /L <br />0.14 <br />97 <br />70 130 <br />0.0 <br />20 <br />Calcium <br />606 mg /L <br />1.0 <br />97 <br />70 130 <br />2.0 <br />20 <br />Iron <br />11.3 mg /L <br />0.030 <br />99 <br />70 130 <br />0.4 <br />20 <br />Magnesium <br />511 mg /L <br />1.0 <br />96 <br />70 130 <br />0.2 <br />20 <br />Manganese <br />10.3 mg /L <br />0.0024 <br />95 <br />70 130 <br />1.1 <br />20 <br />Potassium <br />456 mg /L <br />1.0 <br />88 <br />70 130 <br />1.5 <br />20 <br />Zinc <br />9.72 mg /L <br />0.025 <br />95 <br />70 130 <br />0.2 <br />20 <br />Method: <br />E200.7 <br />Analytical Run: ICP2- C_131125E <br />Sample ID: <br />ICV <br />Initial Calibration Verification Standard <br />11/25/13 13:45 <br />Sodium <br />51.8 mg /L <br />0.50 <br />104 <br />95 105 <br />Sample ID: <br />ICSA <br />Interference Check Sample A <br />11/25/13 14:32 <br />Sodium <br />- 0.0974 mg /L <br />0.50 <br />Sample ID: <br />ICSAB <br />Interference Check Sample AB <br />11/25/13 14:36 <br />Sodium <br />0.0247 mg /L <br />0.50 <br />Method: <br />E200.7 <br />Batch: R181220 <br />Sample ID: <br />MB- 131125A <br />Method Blank <br />Run: ICP2- C_131125E <br />11/25/13 15:00 <br />Sodium <br />ND mg /L <br />0.3 <br />Sample ID: <br />LFB- 131125A <br />Laboratory Fortified Blank <br />Run: ICP2- C_131125E <br />11/25/13 15:04 <br />Sodium <br />49.8 mg /L <br />0.50 <br />100 <br />85 115 <br />Sample ID: <br />C13110305- 001CMS2 <br />Sample Matrix Spike <br />Run: ICP2- C_131125E <br />11/26/13 00:49 <br />Sodium <br />114 mg /L <br />1.0 <br />100 <br />70 130 <br />Sample ID: <br />C13110305- 001CMSD2 <br />Sample Matrix Spike Duplicate <br />Run: ICP2- C_131125E <br />11/26/13 00:53 <br />Sodium <br />115 mg /L <br />1.0 <br />101 <br />70 130 <br />0.5 20 <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />ND - Not detected at the reporting limit. <br />Page 13 of 30 <br />