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ACZ Laboratories, Inc. <br />2773 Dnwnhdl r)nve Steamhnat Snnnns Cn Rn4R7 tRnn) .144- 5491 <br />Star Mine Operations LLC <br />Project ID: <br />Sample ID: MW -1 <br />Wet Chemistry <br />ACZ Sample ID <br />Date Sampled <br />Date Received <br />Sample Matrix <br />L14706-01 <br />09126113 11:15 <br />09/27/13 <br />Waste Water <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 3 of 27 <br />imution <br />Kesuit <br />Qual <br />AQ a n its <br />K.DL <br />PQL <br />Date Analyst <br />Fluoride <br />Alkalinity as CaCC3 <br />SM2320B- Titration <br />0.2 B * <br />mg /L <br />0.1 <br />0.5 <br />10/08/1317.44 <br />khw <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />Bicarbonate as <br />118 <br />1 <br />55 <br />7 <br />mg /L <br />2 <br />20 <br />09/28/13 0 00 <br />mss3 <br />CaCO3 <br />10/04/13 11.10 <br />id <br />filter) <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />09/28/13 0,00 <br />mss3 <br />Hydroxide as CaCO3 <br />1 <br />mfm <br />U <br />mg /L <br />2 <br />20 <br />09/28/13 0:00 <br />mss3 <br />Total Alkalinity <br />1 <br />55 <br />M353 2 - H2SO4 preserved <br />mg /L <br />2 <br />20 <br />09/28/13 0 00 <br />mss3 <br />Cation -Anion Balance <br />Calculation <br />pH (lab) <br />SM4500H+ B <br />Cation -Anion Balance <br />pH <br />4.0 <br />8.2 H <br />% <br />0.1 <br />0.1 <br />10/16/13 1024 <br />talc <br />Sum of Anions <br />1 <br />2.4 <br />C <br />meq /L <br />0.1 <br />0.5 <br />10/16/13 10.24 <br />talc <br />Sum of Cations <br />1 <br />0.01 B <br />2.6 <br />0.01 <br />meq /L <br />0.1 <br />0.5 <br />10/16/13 10 24 <br />talc <br />Chloride <br />SM4500CI -E <br />1 <br />U <br />* mg /L <br />1 <br />5 <br />10/10/1312:04 <br />mpb <br />Conductivity @25C <br />SM2510B <br />1 <br />276 <br />10/01/13 14.33 <br />* umhos /cm <br />1 <br />10 <br />09/28/13 3:39 <br />mss3 <br />Cyanide, total <br />M3354- Colonmetncw /distillation <br />0.5 <br />U <br />mg /L <br />0.003 <br />0.01 <br />10/09/13 13:38 <br />mpb <br />Cyanide, WAD <br />SM4500 -CN I- Colorimetrlc <br />0.5 <br />mss3 <br />U <br />* mg /L <br />0.003 <br />0.01 <br />10/09/13 1501 <br />mla <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 3 of 27 <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.2 B * <br />mg /L <br />0.1 <br />0.5 <br />10/08/1317.44 <br />khw <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />118 <br />mg /L <br />1 <br />7 <br />10/16/13 10.24 <br />talc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />10/04/13 11.10 <br />id <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />09/30/13 13.41 <br />mfm <br />& Acidification <br />Nitrate /Nitnte as N <br />M353 2 - H2SO4 preserved <br />1 <br />1.56 <br />mg /L <br />0.02 <br />0.1 <br />10/04/13 23.40 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.2 H <br />units <br />0.1 <br />0.1 <br />09/28/13 0.00 <br />mss3 <br />pH measured at <br />1 <br />21 <br />C <br />0.1 <br />0.1 <br />09/28/13 0:00 <br />mss3 <br />Phosphorus, ortho <br />M365 1 -Automated Ascorbic Acid <br />1 <br />0.01 B <br />mg /L <br />0.01 <br />0.05 <br />09/27/13 22:12 <br />pjb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />174 <br />mg /L <br />10 <br />20 <br />10/01/13 14.33 <br />mss3 <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />185 <br />mg /L <br />5 <br />20 <br />10/02/13 14:53 <br />mss3 <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516 -02 - Turbidimetnc <br />5 <br />62.0 <br />mg /L <br />5 <br />25 <br />10/08/13 17.12 <br />tcd <br />TDS (calculated) <br />Calculation <br />153 <br />mg /L <br />10 <br />50 <br />10/16/13 10.24 <br />talc <br />TDS (ratio - <br />Calculation <br />1,14 <br />10/16/13 10:24 <br />talc <br />measured /calculated) <br />For Cadmium by <br />ICPMS, the value in the MDL <br />field is the client's requested <br />reporting limit. <br />A "U" qualifier denotes <br />cadmium was not detected above this level. <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 3 of 27 <br />