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ADZ Laboratories, Inc. <br />9773 0nwnhdl r)nve StParnhnat .Snnnrrs r r) Rn4R7 /Rnni .4.44 -54Q.4 <br />Star Mine Operations LLC ACZ Sample ID: <br />L14706 -03 <br />Project ID: Date Sampled: <br />09126113 12:15 <br />Sample ID: MW -3 Date Received: <br />09127113 <br />Sample Matrix: <br />Waste Water <br />Wet Chemistry <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 7 of 27 <br />ivution <br />Kesuit <br />Qual AQ <br />Inits <br />MDL <br />R <br />Date <br />Fluoride <br />Alkalinity as CaCO3 <br />SM2320B - Titration <br />0.1 B * <br />mg /L <br />0.1 <br />0.5 <br />10/08/1317.59 <br />khw <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />Bicarbonate as <br />113 <br />1 <br />53 <br />7 <br />mg /L <br />2 <br />20 <br />09/28/13 0:00 <br />mss3 <br />CaCC3 <br />10/04/13 11.18 <br />id <br />filter) <br />Carbonate as CaCO3 <br />1 <br />U <br />mg /L <br />2 <br />20 <br />09/28/13 0.00 <br />mss3 <br />Hydroxide as CaCO3 <br />1 <br />mfm <br />U <br />mg /L <br />2 <br />20 <br />09/28/13 0.00 <br />mss3 <br />Total Alkalinity <br />1 <br />53 <br />M353 2 - H2SO4 preserved <br />mg /L <br />2 <br />20 <br />09/28/13 0 00 <br />mss3 <br />Cation -Anion Balance <br />Calculation <br />pH (lab) <br />SM4500H+ B <br />Cation -Anion Balance <br />pH <br />351 <br />8.2 H <br />% <br />0.1 <br />0.1 <br />10/16/13 10:24 <br />talc <br />Sum of Anions <br />1 <br />1.2 <br />C <br />meq /L <br />0.1 <br />0.5 <br />10/16/13 10:24 <br />talc <br />Sum of Cations <br />1 <br />U <br />2.5 <br />0.01 <br />meq /L <br />0.1 <br />0.5 <br />10/16/13 10 24 <br />talc <br />Chloride <br />SM45000I -E <br />1 <br />U <br />mg /L <br />1 <br />5 <br />10/10/1312.04 <br />mpb <br />Conductivity @25C <br />SM2510B <br />1 <br />265 <br />10/01/13 14.35 <br />umhos /cm <br />1 <br />10 <br />09/28/13 3.55 <br />mss3 <br />Cyanide, total <br />M3354- Colonmetncw /distillation <br />0.5 <br />U * <br />mg /L <br />0.003 <br />0.01 <br />10/09/13 13.40 <br />mpb <br />Cyanide, WAD <br />SM4500 -CN I- Colonmetric <br />0.5 <br />id <br />U * <br />mg /L <br />0.003 <br />0.01 <br />10/09/13 15:04 <br />mla <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 7 of 27 <br />w/ distillation <br />Fluoride <br />SM450OF -C <br />1 <br />0.1 B * <br />mg /L <br />0.1 <br />0.5 <br />10/08/1317.59 <br />khw <br />Hardness as CaCO3 <br />SM2340B - Calculation <br />113 <br />mg /L <br />1 <br />7 <br />10/16/13 10 24 <br />talc <br />Lab Filtration (0.45um <br />SOPWC050 <br />1 <br />10/04/13 11.18 <br />id <br />filter) <br />Lab Filtration (0.45um) <br />M200.7/200.8 <br />1 <br />09/30/13 13:42 <br />mfm <br />& Acidification <br />Nitrate /Nitrite as N <br />M353 2 - H2SO4 preserved <br />1 <br />0.34 <br />mg /L <br />0.02 <br />0.1 <br />10/04/13 23.45 <br />pjb <br />pH (lab) <br />SM4500H+ B <br />pH <br />1 <br />8.2 H <br />units <br />0.1 <br />0.1 <br />09/28/13 0.00 <br />mss3 <br />pH measured at <br />1 <br />21 <br />C <br />0.1 <br />0.1 <br />09/28/13 0:00 <br />mss3 <br />Phosphorus, ortho <br />M365 1 - Automated Ascorbic Acid <br />1 <br />U <br />mg /L <br />0.01 <br />0.05 <br />09/27/13 22:15 <br />plb <br />dissolved <br />Residue, Filterable <br />SM2540C <br />1 <br />164 <br />mg /L <br />10 <br />20 <br />10/01/13 14.35 <br />mss3 <br />(TDS) @180C <br />Residue, Non- <br />SM2540D <br />1 <br />8 B <br />mg /L <br />5 <br />20 <br />10/03/13 10:07 <br />id <br />Filterable (TSS) <br />@105C <br />Sulfate <br />D516- 02- Turbidimetnc <br />1 <br />5.5 <br />mg /L <br />1 <br />5 <br />10/08/1317.04 <br />tcd <br />TDS (calculated) <br />Calculation <br />92 <br />mg /L <br />10 <br />50 <br />10/16/13 1024 <br />talc <br />TDS (ratio - <br />Calculation <br />1,78 <br />10/16/13 10:24 <br />talc <br />measured /calculated) <br />For Cadmium by ICPMS, the value in the MDL <br />field is the client's requested <br />reporting limit. <br />A "U" qualifier denotes cadmium was not detected above this level. <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details <br />Page 7 of 27 <br />